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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> r McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mLe bell com E-mail main@mccampbell corn
<br /> rAdvanced GeoEnvironmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01
<br /> r 837 Shaw Road Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01
<br /> r Client P O Date Analyzed 12/04-12/07/01
<br /> Volatile Organzes By GC/MS
<br /> EPA method 8260
<br /> r Lab ID 84504
<br /> Client ID P16(36-40)/1 12901
<br /> Matrix W
<br /> r Reporting Limit Reporting Limit
<br /> W S
<br /> Compound Concentration* Compound Concentration* W 5 �
<br /> Acetone[bi ND<10 50 25 trans-l,3-Dichlorcpropene ND 10 50
<br /> Benzene ND to 50 Ethylene dibromide ND 1 0 50
<br /> r Bromobenzene ND 10 5 0 Ethylbenzene ND 1 0 5 0
<br /> Bromochloromethane ND 10 5 0 Hexachiorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 1 0 50 lodomethane ND l 0 5 0
<br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND l 0 50
<br /> r Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 5 0
<br /> n-Butyi benzene ND 1 0 50 Methyl butyl ketone ND € 0 0
<br /> sec-Butyl benzene ND 10 50 1 Methylene Chloride"' ND<5 0 1 1 0 50
<br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone M ND 1 2 0 10
<br /> Carbon Disuifde ND 10 50 Methyl isobutyl ketone g' ND 1 0 50
<br /> Carbon i etrachlonde ND 1 0 50 Methyl tent-Butyl Ether(MTBE) 1 0 50
<br /> Chlorobenzene ND 10 50 Naphthalene ND 5 0 25
<br /> Chloroethane ND t 0 5 0 n-Propyl benzene ND 1 0 50
<br /> r 2-Chloreethyl Vinyl Ether"' ND 1 0 5 0 Styrene ND l 0 € 5 0
<br /> Chloroform ND 10 5 0 1,1,1,2-Tetrac.hioroethane ND 1 0 5 0
<br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 1 0 5 0
<br /> r 4-Chlorotoluene ND 10 5 0 Toluene ND 1 0 5 0
<br /> Dibromochloromethane ND 1 0 50 1,2,3-Trichlombenzenc ND 1 5 0 25
<br /> I,2-Dibromo-3-chloropropane ND 20 10 1,2 4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND l 0 5 0 1,1,1-Trichloroethane ND 1 0 50
<br /> r 1,2-Dichlorobenzene ND to 5 0 1,1 2-Trichloroethane ND 1 0 50
<br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 1 0 50
<br /> i,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 5 0
<br /> Dichlorodifluoromethane ND 10 5 0 1,2 3-Trichloropropane ND 1 0 50
<br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 1 0 50
<br /> 1,2-Dichloroetharie ND 10 5 0 1 3,5-Tnmethylbenzene ND l 0 5 0
<br /> IJ-Dichloroethene ND 10 50 Vinyl Acetate m ND 5 0 25
<br /> cis-l,2-Ehchloroethene ND 10 5 0 Vinyl Chlonde ° ND 1 0 5 0
<br /> trans-l,2-Dichloroethene ND to 5 0 Xylenes,total ND 1 0 50
<br /> 1,2-Dichloropropane ND 10 5 0 1 Comments
<br /> 1 3-Dichloropropane ND 10 50 1 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 50 Dibromolluoromethane 97
<br /> 1,1-Dichloropropene ND 10 5 0 Toluene-dg 109
<br /> cis-1,3-Dichloropropene ND 10 5 0 4-Bromotluorobenzene 107
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> . (b) 2-prupanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (1i) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene (m) acetic acid ethenyl ester, (n)
<br /> chloroethenc,(o)dimethylbenzenes
<br /> DHS Certification No 1644 LAP dward Hamilton, Lab Director
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