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110 2nd Avenue South,#D7, Pacheco, CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 CIient Contact Tim Cuellar Date Extracted 12/04-12107/01 <br /> IClient P O Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84505 <br /> Client ID P16(96-100)/112907 <br /> Matrix W <br /> Reporting Limit Reporting Umrt <br /> Compound Concentration* Reporting <br /> S Compound Concentration* Reporting <br /> S <br /> Acetone the ND<10 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 50 <br /> Bromobenzene ND 1 6 5 0 Ethylbenzene ND 1 4 50 <br /> Bromochloromethane 'dD 1 0 50 Hexachlorobutadiene ND 5 0 25 <br /> Bromodtchloromethane ND 1 D 5 0 Iodomethane ND 1 0 50 <br /> Bromotorm ND to 50 Isopropy€benzene ND 1 0 50 <br /> Bromomelhane ND —to 50 p-lsopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride") ND<5 0 l 0 50 <br /> • tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone Lhu ND 1 0 50 <br /> Carbon Tetrachlonde ND 10 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 0 50 <br /> 2 Chloroethyl Vinyl Ether ' ND 10 50 Styrene ND 1 0 50 <br /> Chloroform ND 10 50 1,11,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 50 1 1,2,2-Tetrachloroethane ND 1 0 5O <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 10 50 <br /> 4-Chlorotolume ND to 50 Toluene ND l 0 50 <br /> Dibromochloromethane ND to 50 1 2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropmpane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br />' Dibramornethane ND 10 50 1,1,1-Trichloroethane ND 10 50 <br /> 1 2-Dichlorobenzene ND 1 0 50 1,1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane ND 1 0 50 <br /> 1,1-1)ichloroethane ND 1 0 50 1,2,4-Trimethylbenzene ND 1 0 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 1 0 50 <br /> l,1-Dichloroethene ND 10 50 Vinyl Acetate m ND 50 25 <br />' cis-1,2-Du,hloroethene ND 10 50 Vinyl Chloride " ND 1 0 5 0 <br /> trans-I 2-Diehl oroethene ND 10 50 Xylenes,total ND 1 0 S D <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br />' 2 2-Dichloropmpane ND l 0 50 Dibromotluoromethane 106 <br /> l l-Dichloropropene i 1 0 5 4 Toluene-d8 110 <br /> cis-1 3-Dichloropropene ND 1 0 S D 4-Sromofluorobenzene 107 <br />' .water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting lirrut,N/A means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-heranone (e) dichloromethane, (0 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br />' sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />