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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCA_MPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell coin E-mail main@mccarnpbell com <br /> Advanced GeoEnvtronmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br />' Stockton, CA 95215 Client Contact Tian Cuellar Date Extracted 12/04-12/07/01 <br /> Client P G Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By CCIMS <br /> EFA method 8260 <br /> Lab 1D 84506 <br /> Client 1D P 16(76-80)1112901 <br /> Matrix W <br /> Repomng Limit Rcporhng Limit <br /> Compound Concentration* W S Compound Concentration* w 5 <br /> Acetone ioi ND<10 50 25 trans-1,3-Dtchloropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 50 <br />' Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromocbloramethane ND 1 0 50 Hexachlorobutadiene ND 5 D 25 <br /> Bromodichioromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND 1 0 50 <br />' Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND —10 56 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND i 0 5 0 <br /> pec-Butyl benzene ND 10 50 Methylene Chlonae" ND<5 0 1 0 50 <br /> tert-Butyi benzene ND 10 50 Methyl ethyi ketone IP ND 20 10 <br /> I. Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ai ND 1 0 50 <br /> Carbon-1etrachlonde ND ...10 50 1+Iethyl ten-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 10 5 0 Naphthaiene ND 5 0 25 <br /> Chloroethane ND 1 0 50 n-Ptopyi benzene ND 1 0 5 0 <br /> 2 Chloroethyl Vinyl Ether" ND 10 5 0 Styrene ND 1 0 5 0 <br /> Chloroform ND 1 0 5 0 1 1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 1 0 5 0 1 1,2,2-Tetrachiorocthane ND i 0 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 fetrachioroethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 10 5 0 Toluene` ND 1 0 5 0 <br /> Dibroinochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-DibroMO-3-Lhloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br />' l 2-Dtchlorobenzene ND 10 5 0 1,1,2-Tnchloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Tnchlorotluoromethane ND 10 5 0 <br /> Dichiorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 1 0 5 0 <br />' l I-Dichloroethane ND 1 0 5 0 1,2,4-Trimethylbenzene ND 1 0 5 0 <br /> 1,2-Diebloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene { ND 1 05 0 <br /> 1,1-Dichloroethene ND 10 i 5 0 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dtchloroethene ND 1-07, 5 0 Vinyl Chloride ° ND 1 0 5O <br /> trans-l,2-Dtchloroethene ND 10 5 0 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries <br /> 2,2-Dichioropropane ND 10 5 0 Dibromoiluoromethane 108 <br /> I l,l-Dtchloropropene ND 10 5 0 Toluene-d8 109 <br /> cis-1,3-Dtchloropropene ND 10 5 0 4-Bromofluorobenzene 106 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLA extracts in ug/L <br />' ND means not dctected above the reporting hrrut,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyi ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropy[acetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than—5 vol % <br />' sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, {1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />