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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> httn//www mccamybeil corn E-mail main@mccampbell corn
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<br />' Advanced GeoEnvtronmental Client Project ID Three B's Date Sampled 11/30/01
<br /> 837 Shaw Road Date Received 12/04/01
<br />' Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/07-12/11/01
<br />' Client P O Date Analyzed 12/07-12/11/01
<br /> Volatile Organics By GC/MS
<br /> EPA method$260
<br />' Lab ID 84745
<br /> Client ID P17(91-96)/113001
<br /> Matrix W
<br /> * Reporting Limit Reporting Limit
<br /> Compound Concentration W S Compound Concentrations'
<br /> W S
<br /> Acetone(b) ND<10 50 25 trans-1,3-Dichloropropene ND 1 0 50
<br /> Benzene 27 10 50 Ethylene dibromtde ND 1 0 50
<br /> Bromobenzene ND 10 50 Ethyibenzene 1 7 1 0 50
<br /> Bromochioromethane ND 1 0 50 HexachIorobutadtene ND 50
<br /> Bromodichloromethane ND 1 0 50 lodomethane ND 1 0
<br /> Bromofonn ND 10 50 Isopropylbenzene ND 1 0
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 51
<br /> I n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 5 0
<br /> sec-Butyl benzene ND 1 0 50 Methyiene Chloride"' ND<2 0 1 0 5 0
<br /> tert-Butyi benzene ND 10 50 Methyl ethyl ketone ND 20 ]0
<br />�. Carbon Disulfide ND 10 50 Methyl isobutyt ketone ND 1 0 5 0
<br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 1 0 5 0
<br /> Chlorobenzene ND 10 50 Naphthalene 94 50 25
<br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 0 5 0
<br /> 2-Chloroethyl Vinyl Ether"I ND 1 0 50 Styrene ND 1 0 5 0
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachioroethane ND 10 50
<br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 1 0 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 1 6 1 0 50
<br /> Dibromochloromethane ND 1 0 50 1 2,3-Trrchlorobenzene ND 50 25
<br /> 1,2-Dibromo-3-chioropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 10 50 1,1,]-Trichloroethane ND 10 50
<br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnehloroethane ND 1 0 50
<br /> 1,3-Dichlorobenzene ND 1 0 50 Tnchlomethene ND 1 0 50
<br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 50
<br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnehloropropane ND 1 0 50
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<br /> 1,1-Dichloroethane ND 0 50 1 2,4-Tnmethylbenzene 40 1 0 50
<br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 1 0 so
<br /> IJ-Dichioroethene ND 1 0 50 Vinyl Acetate m - ND 50 25
<br /> c3s-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride t"' ND 1 0 50
<br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total 65 1 0 50
<br /> 1,2-Dechloropropane ND 10 50 Comments
<br /> 1,3-Dechloropropane ND _10 —To— Surrogate Recoveries(%)
<br /> 2 2-Dechloropropane ND 1 0 50 Dibromotluoromethane 101
<br /> 1,1-Dichloropmpene ND 1 0 50 Toluene-d8 98
<br /> cis-i,3-Dichloropropene ND L 0 50 4-Brome luorobenzene 94
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in uWwipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts
<br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> • pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than –5 vol %
<br /> sediment, {1) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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