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110 2nd Avenue South, #D7,Pacheco,CA 94553-5560
<br />' MCCAIMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> . http//www mccampbell com E-mail main@,mccampbell com
<br />' Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/30/01
<br />' 837 Shaw Road Date Received 12/04/01
<br /> Stockton, CA 95215 Client Contact Tirn Cuellar Date Extracted 12107-12/11/01
<br />' Client P O Date Analyzed 12/07-I2/11/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br />' Lab ID 84746
<br /> Client ID P17(117-120)/113001
<br /> Matrix W
<br /> * Reporting L=mit Rcportmg Limit
<br /> W S
<br /> Compound Concentration Compound Concentration*
<br /> VV S
<br /> Acetone tui ND<10 50 25 trans-l,3-Dtchloropropene ND 1 0 50
<br /> Benzene 1 8 ] 0 50 Ethylene dibromide ND 1 0 50
<br />' Bromobenzene NO 1 0 5 0 Ethylbenzene 3 0 1 D 50
<br /> Bromochloromethane ND €0 50 Hexachlorobutadime ND 50 25
<br /> Bromodichloromethane ND l 0 50 lodomethane ND 1 0 5 0
<br /> Bromolorm ND 1 0 5 0 Isopropylbenzene ND 1 0 50
<br />' Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 50
<br /> n-Butyl benzene 12 10 5 0 a Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 1 0 5 0 1 Methylene Chloride e ND<2 0 1 0 5 0
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 1 0 5 0 Methyl isobuty]ketone' ND 1 0 5 0
<br /> lie
<br /> Carbon Tetrachloride ND 10 5 0 Methyl tert-Butyl Ether(MTBE) 1 0 50
<br /> Chlorobenzene ND 1 D 50 Naphthalene 15 5 0 25
<br /> Chloroethane ND 1 0 50 n-Propyl benzene 1 3 1 0 5 0
<br /> 2-Chloroethyl Vinyl Ether" ND 1 0 5 0 Styrene ND l 0 50
<br /> Chloroform ND 1 4 5 0 1 1 1,2-Tetrachloroethane ND 1 0 5 0
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 50
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethane ND 1 0 50
<br /> 4-Chlorotoluene ND 10 1 5 0 Toluene 1 7 1 0 5 0
<br /> Dibromochloromethane ND 10 50 1,2,3-Trichlorobenzene ND 5 0 25
<br /> 12-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 10 5 0 1,1,1-Trichloroethane ND 1 0 5 0
<br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Trichloroethane ND 1 0 50
<br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 1 0 50
<br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlorefluoromethane ND 10 5 0
<br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnehloropropane ND 1 0 50
<br /> 1,1-Dichloroethane ND 14 50 1,24-Tnmethylhenzene 14 ] 0 54
<br /> 1 2-Dichloraethane ND 10 5 0 1,3 5-Tnmethylbenzene 2 1 10 50
<br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate m' ND 50 25
<br /> cis-1,2-Dichloroethene ND 1 0 5 4 Vinyl Chloride ° ND 1 D 5 0
<br /> trans-1,2-Dichloroethene ND to 5 0 Xylenes,total 12 1 0 11 5 0
<br /> 1,2-Dichloropropane ND 1 0 50 Comments h
<br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries
<br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 141
<br /> 1 1-Dichloropropene ND 10 5 0 Toluene-d8 98
<br /> cis-1,3-Dichloropropene ND 1 0 5 0 4-Bromofluorobenzene 94
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than —5 voi %
<br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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