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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 1 httn//www mccampbell com E-mail main@mccampbell com <br /> • <br />' Advanced GeoEnvtronmental Client Project ID Three B's Date Sampled 11/30/01 <br />' 837 Shaw Road Date Received 12/04/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br />' Client P O Date Analyzed I2/07-12111/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84749 <br /> Client ID P18(72-76)/113001 <br /> Matrix W <br /> Compound Concentration* RWmng Limit <br /> Compound Concentrauon* R p rtes Limit <br /> I <br /> Acetone'�1 ND<10 5 0 25 trans-1 3-Dichlompropene ND 1 0 50 <br /> Benzene ND l 0 50 Ethylene dibromide ND 1 0 50 <br />' Bromobenzene ND l 0 50 Ethylbenzene ND 1 0 �0 <br /> Bromochloromethane ND 1 0 30 Herachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 1 0 D 0 <br /> Bromoform ND 1 0 50 Isopmpylbenzene ND 1 0 50 <br />' Bromomethane ND 1 0 50 p-lsopropy€toluene ND -10 50 <br /> n-Butyl benzene ND 10 50 Methyl butyi ketone ND 1 0 50 <br /> sec Butyl benzene ND 10 50 Methy€enc Chlonde` ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketoneND 20 10 <br />' Carbon Disulfide ND l 0 50 Methyl isobutyl ketone 18 ND 1 0 5 0 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tett-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 10 30 Naphthalene ND 50 25 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether` ND 10 50 Styrene ND to 50 <br /> Chloroform ND 10 50 1,1,12-Tetrachloroethane ND l0 50 <br /> Chloromethane ND 1 0 V1,23-Tnehlarobertzme <br /> -Tc trichloroethane ND 1 0 50 <br /> 2-Chlorotoiuene ND 1 0 loroethene ND 1 0 50 <br /> 4-Chlorotoiuene ND 10 e ND 1 0 50 <br /> Dibromachloromethane ND to nchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chlompmpane ND 20 nchlorobenzene ND 50 2�Dibromornethane ND 10 richloroethane ND 1 0 3 0 <br />' 1 2-Dichiorobenzene ND l 0 50 1,1,2-Tnchloroethane ND 1 0 3 0 <br /> 1,3-Dichlorobenzene AND 10 50 Trichloroethene ND 1 0 5 0 <br /> 1 4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 50 <br /> achlorodifluoromethane ND 10 50 l 2,3-Trichloropropane ND 10 50 <br />' 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethy€benzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 1 0 50 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate °` ND 50 25 <br /> cis-1,2-Dichloroethene ND I Q 50 Vinyl Chloride n ND 1 0 50 <br /> trans-1 2-Dichloroethene ND 10 50 Xylenes,total ND 1 0 S Q <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 102 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND 10 I 4-$tomo€luorobenzene 94 <br /> `water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting haat,N/A means analyte not applicable to thts analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (1)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chlomethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 JIF Edward Hatnilton,Lab Director <br /> I <br />