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_ x <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' F14 McCANIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@mccampbell com <br /> Advanced GeoE2ivironmental Client Project ID Three B's Date Sampled 11/30/01 <br /> 837 Shaw Road Date Received 12/04/01 <br /> Stockton, CA 95215 CIient Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br />' <br /> [Client P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' <br /> Lab ID 84748 <br /> Client ID P18(42-46)/113001 <br /> Matnx W <br /> Reporung Limt Rgmrdng Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone °J ND<10 so 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 5 0 <br />' Bromoberizene ND 10 50 Ethylbenzene ND 1 0 5 D <br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 10 5 0 i <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 10 50 <br />' Bromomethane ND 10 50 p4sopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone' ND l 0 50 <br /> bec-Butyl benzene ND 10 50 Methylene Chlondet` ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10 <br />'• Carbon Disulfide ND 10 50 Methyl isobutyl ketones ND 10 50 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 50 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND l 0 i 50 <br /> 2-Chloroethyl Vinyl Ether') VD l 0 50 Styrene ND 1 0 5 0 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 a0 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethane ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 50 11 Toluene NO 1 0 50 <br /> Dibromochloramethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chioropropane ND 20 10 €,2 4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroethane ND 1 0 50 <br />' 1,2-Dichlorobenzene ND 10 5 D 1,1 2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichiorobenzene ND 1 0 50 Tnchlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchioropropane ND 1 0 50 <br />' t,l-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 1 D 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 1 0 50 <br /> IJ-Dichloroethene ND 10 50 Vinyl Acetate m' LJE <br /> D 5 0 25 <br /> cis-1,2-Dichloroethene ND 3 0 50 Vinyl Chloride ") 1 0 50 <br /> trans-l,2-Dichloroethene ND 1 0 50 Xylenes,total 1 0 5 0 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 103 <br /> ],I-Dichloropropene ND 10 50 Toluene-l8 98 <br /> cis-1,3-Dichloropropene ND 1 D 5 0 4-Btnmofluombenzene 95 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> • (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> I sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />