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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail mainQa mccampbell com <br /> Date Sampled 11/26-11/27/01 <br /> Advanced GeoEnvironmental Client Pro3ect ID Three B's <br /> Date Received 11/30/01 <br /> 837 Sbaw Road <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 12103-12106/01 <br /> Client P O Date Analyzed 12/03-12/06101 <br /> IVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84511 <br /> Client ID CPT13(16-20)/1 12601 <br /> Matrix W <br /> Report=ng Limit R"mng Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone'b NLK15 50 25 trans-1 3-Dichloropropene ND 1 0 5 0 <br /> Benzene ND 10 5 D i Ethylene dibromide ND 1 0 5 0 <br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND to 50 <br />' Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND —To­ 5 0 Iodomethane ND 10 5 0 <br /> Bromoform ND 1 D 5 D Isopropylbenzene ND 10 5 0 <br /> Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 .50 Methyl butyi ketone i ND 10 5 0 <br /> sec-Butyl benzene ND t 0 5 0 Methylene Chloride' ND<2 0 10 5 0 <br /> tent-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND2 0 10 <br /> Carbon Disulfide ND 10 --3-0 Methyl isobutyl ketone ND 10 5 0 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tett-Butyl Ether(MTBE) -- 10 5 0 <br /> Chlorobenzene ND 1 0 —50 Naphthalene ND 5 0 25 <br /> S D n-Propyl benzene ND <br /> Chloroethane ND 10 1 0 5 0 <br /> 2-Chloroethyl Vinyi Ether" ND I O5 0 Styrene ND 10 <br /> 5 0 <br /> 1 Chloroform ND 10 5 0 1 1,1 2-Tetrachloroethane ND 1 0 5 U <br /> Chloromethane ND 1 0 5 0 1,1 2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chiorotoiuene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 D <br /> 4-Clilorotoluene ND 1 0 5 0 Toluene ND 10 5 0 <br /> Dibromochlorornethane ND 1 0 --5-o 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND f-0— 10 1,2,4-Tnehlorobenzene ND 5 0 25 <br /> Dibromornethane ND 1 0 5 0 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 10 U <br /> 1,3-Dichlorobenzene ND 1 0 _7_0 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 10 5 0 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND <br /> 10 5 0 1,2,3-Tnchloro nopane ND 1 0 5 0 <br /> 0 <br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 1 0 5 0 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 1 50 <br /> 1,i-Dichloroethene ND 10 __5_O_ Vinyl Acetate "' ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride ' ND l 0 5 D <br /> trans-l,2-Dichlorocthene ND 10 5 0 J{ylenes,total ND 1 0 5 0 <br /> 1,2-Dtchloropropane ND 1 0 5 D Comments <br /> 1,3-Dichloropropane ND 1 p —50 Surrogate Recoveries <br /> 2,2-Dtchloropropane ND 1 0 50 Dibromofluoromethane 87 <br /> 1 1-Dichloropropene ND 10 5 0 Toluene-d8 117 <br /> cis-1,3-Dichloropropene ND 10 5 0 4-Bromotluorobenzene 100 <br /> �j <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentarione or isopropylacetone,(h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than—5 vol % <br /> sediment, 6) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward$amilton,Lab Director <br /> 1 <br />