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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL NC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell corn E-mail main@mccampbell cam <br /> Date Sampled 11/26-11/27/01 <br /> Advanced GeoEnvlronnental Client Project ID Three B's <br /> Date Received 11/30/01 <br /> 837 Shaw Road <br />' Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12103-12/06/01 <br /> Client P 0 Date Analyzed 12/03-12/06/01 <br />' Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 84512 <br />' Client 1D CPT13(38-42)1112601 <br /> Matrix W <br /> Repotung Limit * Repomng Limit <br /> Compound Concentration* W S Compound Concentration T05 <br />' Acetone tsi ND<15 50 25 trans-l,3-Dichloropropene ND <br /> Benzene ND 1 0 __5O_ Ethylene dibromide VD <br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND Bromodichloromethane ND l0 50 ladomethane ND Bromotorm ND 1 0 5 0 Isopropylbenzene ND <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 1 0 5 0 <br /> ,-Butyl benzene ND 1 0 50 Methyl butyl ketone ND l 0 5 0 <br /> aec-Butyl benzene ND 1 0 50 Methylene Chloride" 'VD<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 1 0 TO— Methyl ethyl ketone ND i 20 10 <br /> Carbon Disulfide ND to 50 Methyl isobutyl ketone ND 10 5 0 <br /> Caxbon Tetrachloride ND to 5 0 Methyl Cert-Butyl Ether(MTBE) --- 10 50 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 5 0 25 <br /> Chloroethane ND to 50 n-Propyl benzene ND 1 0 5 0 <br /> 2-Caloroethyl Vinyl Ether" ND 1 0 5 0 Styrene ND 1 0 5 0 <br /> Chloroform ND 1 0 5 0 1,1 1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 1-0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotolu me ND 1 0 50 Tetraehloroethene ND 1 0 5 0 <br /> 4-Chlorotoiuene ND 10 50 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Trichlorabenzene [+ID 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 lU 1,2,4-Tneblorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 0 5 0 1,1,1-Trichloroethane ND 10 50 <br /> 1,2-Dichloro3enzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 10 5 0 Trichlorofluoromethane ND 10 50 <br /> Dtchlorodifluoromethane ND 10 S_0_ 1,2,3-Tnchloropropane ND 10 1 5 0 <br /> l,1-Dichloroethane ND to 5 0 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethyibenzene ND 10 5 0 <br /> 1 1-Dichloroethene ND 10 5 D Vinyl Acetate n _ ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chlonde ° ND 10 5 0 <br /> trans-1,2-Dichloroethene ND 10 5 0 Xylenes total ND 10 1. 5 0 <br /> 1,2-Dtchloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dlbromofluoromethane 115 <br /> l,l-Dichloropropene ND 10 50 Toluene-d8 123 <br /> cis4,3-0ichloropropene ND 1 D 11 5 0 4-Bromofluorobenzene 99 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in uglL <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> ' (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water tnimiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> 1 chioroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />