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110 2nd Avenue South,#137,Pacheco, CA 94553-5560 <br /> McCA1MPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> J4 h"//www mccampbell corn E-mail main@mccampbell cam <br /> Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O I Date Analyzed 12/03-12/06/01 <br /> Volatile Orgamcs By GC/MS <br /> EPA method 8260 <br /> Lab ID 84514 <br /> Client ID CPT13(96-100)/112601 <br /> Matrix W <br /> Repomng Limit Repomng Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone " ND<15 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 1 0 50 Ethylene dibrorrnde ND 10 5 0 <br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 10 5 0 Hexachlorobutadiene ND 1 5 0 25 <br /> Bromodrehloromethane ND 1 0 5 0 lodomethane ND 10 50 <br /> Bromotorm ND 1 0 5 0 Isopropylbenzene ND 1 0 5 0 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene AFD 1 0 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone i ND 1 0 5 0 <br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride(-) ND<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 J 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone'-91 ND 1 0 5 0 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) 1 0 5 0 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 10 5 0 <br /> 2 Chloroethyl Vinyl Ethe ND 1 0 5 0 Styrene ND 10 50 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 10 50 <br />' 4-Chlorotoluene ND 10 5 0 Toluene ND 10 50 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1 1,2,4-Tnehlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 50 <br />' 1,2-Dichlorobenzene ND 1 0 50 1 1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Tnchloroethenc ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 10 5 0 Tnchlorofluommethane ND 10 5 0 <br /> Dichlorodtfluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 10 50 <br />' 1,1-Dichloroethane ND 1 0 5 0 1,2 4-Trimethylbenzene ND 10 5 0 <br /> 1,2-Dichloroethane ND 1 0 50 1,3 5-Tnmethylbenzene ND 10 5 0 <br /> l,]-Dichloroethene ND 1 0 50 Vinyl Acetate 11 - ND 5 0 25 <br /> as-1,2-Dichloroethene ND 10 50 Vinyl Chloride n ND 10 5 0 <br />' trans-1,2-Dichlomethene ND 1 0 50 xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND l 0 5 0 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 5 0 Dibromotluoromethane 116 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 10 5 0 4-Bromofluorobenzene 99 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ugikg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not appheable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> • pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene ( methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chlomethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />