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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www insccampbell com E-mail main@mccampbell com
<br /> tAdvanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01
<br /> 837 Shaw Road Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12103-12/06/01
<br /> Ghent P O Date Analyzed 12/03-12/06/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> I Lab 1D 94513
<br /> Client ID CPT13(76-80)1112601
<br /> Matrix W
<br /> Reporting Limit Repornng Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br /> Acetone 6j ND<15 50 25 trans-l,3-Dichloropropene ND 10 50
<br /> Benzene ND 10 50 Ethylene dibromide ND 10 5 0
<br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50
<br /> Bromochloromethane ND 1 0 5 0 Hexachiorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 1 0 5 0
<br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 1 0 5 0 p-lsopropyl toluene ND 1 0 5 0
<br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 5 0
<br /> sec Butyl benzene ND 1 0 5 0 Methylene Chloridet" ND<2 0 1 0 5 0
<br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone M ND 2 0 10
<br /> Carbon Disulfide ND l 0 5 0 Methyl isobutyl ketone ND 1 0 30
<br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) l 0 50
<br /> ChIorobenzene ND 1 0 5 0 Naphthalene ND 5 0 25
<br /> Chloroethane ND 10 5 0 n-Propyl benzene ND l 0 5 0
<br /> 2-Chloroethyl Vinyl Ether(`) ND 1 0 5 0 Styrene ND 1 0 5 0
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Cblorotoluene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 0
<br /> 4-Chlorotoluene ND 1 0 5 4 Toluene ND 1 0 5 0
<br /> Dibromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> l 2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 5 0 1,1,1-Trichloroethane ND 1 0 5 0
<br /> 1,2-Dichlorobenzene ND i 0 5 0 1,1,2-Trichloroethane ND 10 5 0
<br /> l,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 1 0 5 0
<br /> 1,4-Dichlorobenzene ND 10 5 0 Trichlorofluoromethane ND 1 0 5 0
<br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 10 5 0
<br /> 1,1-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND I O 5 0
<br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 1 0 5 0
<br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate " _ ND 5 0 25
<br /> cis-l,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride In) ND 1 0 5 0
<br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND .10 1 5 0
<br /> 1,2-Dichloropropane ND 1 0 5 0 Comments
<br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries
<br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 115
<br /> 1,1-Dichloropropene ND 10 5 0 Toluene-d8 94
<br /> cis-1,3-Dichloropropene ND 10 50 4-Bromotluorobenzene 100
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting lurut,NIA means analyte not applicable to this analysts
<br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chlomethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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