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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCA1'1/TBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 14 hgR//www mccampbell co m E-mail main@mccampbell cam <br /> Advanced GeoEnviromnental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Read Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O Date Analyzed 12103-12/06/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 84517 <br /> Client 1D CPT]4(39-43)/112701 <br /> Matrix W <br /> Reporting Lvmt Repa=g L�mu <br /> Compound Concentration* W S Compound Concentration* - S <br /> Acetone W ND<15 50 25 trans-1,3 Dichloropropene ND 10 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND to 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromo,-hioromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichioromethane ND 1 0 50 lodomethane ND 1 0 50 <br /> Bromotorm ND 10 50 lsopropylben7ene ND 1 0 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND l 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlonde" ND<2 0 l 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone` ND 20 to <br /> Carbon Disulfide ND 1 0 50 Methvi isobutvl ketone g' ND 1 0 50 <br /> Carbon Tetrachloride ND 1 0 50 Methy€tert-Butyi Ether(MTBE) 10 50 <br /> lie Chlorobenzene ND 1 0 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND to 50 <br /> 2-Chloroethyl Vinyl Ether` ND 1 0 5 0 Styrene ND 10 50 <br /> Chloroform ND 1 0 5 0 1,1,1 2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachioroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 5 0 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 10 —50 <br /> Dibramochloromethane ND 1 0 5 0 1,2 3-Tnehloroben7ene ND 5 0 25 <br /> 1 2-Dibromo-3-chloropropane ND 2 0 10 42 4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Tnchloroethane ND to 50 <br /> 1,2-Dichlorobenzene AFD 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Tnchloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorotluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Trichloropropane ND 10 50 <br />' 1,1-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND 10 5 0 <br /> 1,2-Dichioroethane ND 1 D 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate ' ) - ND 50 25 <br /> cis-1,2-Dtchloroethene ND 1 0 5 0 Vinyl Chloride"" ND 10 5 0 <br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 1 0 50 Dibromatluoromethane 115 <br /> l,]-Dichloropropene ND 10 50 Toluene-d8 115 <br /> cis-1,3-Dichioroprapene VD l U 5 0 4-Bromotluorobenzene 96 <br /> 'water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes m ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting lint,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropy€acetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Harmlton,Lab Director <br />