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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAl\PBELL .ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Iht //www mccamLDbell co m E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road [Ete:-:R:eceived 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O Date Analyzed 12/03-12/06/01 <br /> Volatile Organics By GC/MS <br /> TEP method 8260 <br /> Lab ID 84518 <br /> Client M CPT14(62-67)1112701 <br /> Matrix W <br /> Itepomng Limit Reptutmg Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone(b) N13<15 50 25 trans-I 3-Dtchloropropene ND 10 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND so 25 <br /> Bromodichloromethane ND 10 50 lodomethane ND 1 0 5 0 <br /> Bromoform ND 1 0 50 lsopropylbenzene ND 1 0 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene NO to 50 <br />' n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlondet° ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> lieCarbon Dlsu€flde ND 1 0 50 Methyl isobutyl ketone` ND l 0 50 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND D 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 10 50 <br /> 2-Chioroethyl Vinyl Ether" ND 1 0 50 Styrene ND i 0 50 <br /> Chloroform ND 1 0 50 1,1,1,2-7etrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 -50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chiorotoluene ND 1 0 50 Tetrachloroethene ND 10 50 <br /> 4-Chiorotoluene ND 1 0 50 Toluene ND 10 1 50 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Trichlorobenzene ND S D 25 <br /> 1 2-Dibromo-3-chloropropane ND 20 10 1,2 4-Trichlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 16 50 <br /> 1,2-Dichlorobenzene ND to 50 1,1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnehlorofluoromethane ND 10 50 <br /> Dii.hloroditluoromethane ND 1 0 50 1,2 3-Tnchloropropane ND 10 50 <br /> l,]-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene 12 10 50 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Trimethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate m - ND 50 25 <br /> cis-t,2-ach€oroethene ND I O 50 Vinyl Chloride " ND 1 0 50 <br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ° ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloroproparte ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromotlucromethane 114 <br /> 1,1-Dtchloropropene ND 1 0 50 Toluene-d8 116 <br /> cis-1,3-Dtchloropropene ND 1 0 50 4-Bromofluorobenzene 98 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples to ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting hmu,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chioroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample chat contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />