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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br />' 24 http//www mccampbell co m E-mail main@mccarnpbell com
<br /> Advanced GeoEnvironmentaI Client Protect ID Three B's Date Sampled 11/26-11/27/01
<br /> 837 Shaw Road Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/OI
<br /> Client P O Date Analyzed 12/03-12/06/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br />' Lab M 84520
<br /> Client ID CPT]4(116-119)/112701
<br /> Matrix W
<br /> Rcporting brnu R°p=ng Limit
<br /> Compound Concentration' W S Compound Concentration* W S
<br />' Acetone'b ND<15 50 25 trans-I 3-Dichloropropene ND Io 5 0
<br /> Benzene ND 1 0 50 Ethylene dibrom:de ND 1 0 50
<br /> Bromobenzene ND 1 0 50 Ethyibenzene ND 10 50
<br />' Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25
<br /> Bromodtchloromethane ND 10 50 lodomethane ND 1 0 50
<br /> Bromotorm ND 1 0 50 lsopropylbenzene ND 1 0 1 50
<br /> Bromomethane ND ] 0 50 p-Isopropyl toluene ND 1 0 50
<br />' n-Butyl benzene ND 10 50 Methyl butyl ketone ND 1 D 50
<br /> sec-Butyl benzene ND ] 0 50 Methylene Chloride(.) ND<2 0 10 5 0
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide NO 10 50 Methyl:sobutyl ketune'90 ND 1 0 50
<br /> Carbon Tctrachlonde ND 10 50 Methyl tert-Butyl Ether(MTBE) 1 0 1 5 D
<br /> Chloroberizene ND 10 50 Naphthalene ND 50 25
<br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 10 5 0
<br />' 2-Chloroethyl Vinyl Ether"' ND 1 0 50 Styrene` ND 1 0 5 0
<br /> Chlorotorm ND 1 0 50 l,l,l,2-Tetrachloroethane ND 1 0 5 0
<br /> Chloromethane ND 1 0 50 1 1,2 2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Chlarotoluene ND 1 0 50 Tetrachloroethene ND l 0 50
<br />' 4-Chlorotoluene ND 1 0 50 Toluene ND r10
<br /> 50
<br /> Dibromochloromethane ND l 0 50 1,2,3-Tnchlorobenzene ND 25
<br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 25
<br /> Dibromomethane ND 1 0 50 1 l,]-Trichloroethane ND 50
<br /> 1 1,2-Dtchlorobenzene ND to 50 1,1,2-Trichloroethane ND _.)o
<br /> 1,3-Dichlorobenzene ND l 0 50 Tnchloroethene ND 50
<br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlorofluoromethane ND 50
<br /> Dichlorodifluoromethane ND 1 0 50 l 2,3-Tnchloropropane ND 50
<br />'
<br /> 1,1-Dichioroethane ND 1 0 50 1,2,4-Tnmethvlbenzene ND 5 0
<br /> 1,2-Dichioroethane ND 10 50 1,3,5-Trimethylbenzene ND 10 50
<br /> I,I-Dichloroethene ND 10 50 Vinyl Acetate ND 50 25
<br /> c:s-1,2-Dtchloroethene ND 10- 50 Vinyl Ctilonde ° ND 10 50
<br /> trans-1,2-Dtchloroethene ND 1 0 50 Xylenes,total i° ND 10 50
<br /> 1,2-Dtchloropropane ND l 0 50 Comments
<br /> 1,3-Dichloropropane ND l 0 5 0 Surrogate Recoveries(%}
<br /> 2,2-Dtchloropropane ND 10 50 Dibromofluoromethane 99
<br /> I,1-Dichloropropene ND l0 50 Toluene-d8 105
<br /> cis-l,3-Dtc hloropropene ND i 0 50 4-Bromofluorvbenzene 98
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br />' ND means not detected above the reporting lirmt.NIA means analytc not applicable to this analysis
<br /> (b) 2-proparione or dimethyl ketone, (L) (2 chloroethoxy) etheae (d) 2-hexanone, (e) dichloromethane, (fl 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h) lighter than water tinmiscible sheen is present, (:) liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (lmethylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 V, Edward Hamilton,Lab Director
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