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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4McCA.MPBELL ANALYTICAL, INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ih //www mccam bell com E-mail mai cr mccampbell corn <br /> iAdvanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> iStockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O Date Analyzed 12103-12106/01 <br /> iVolatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 84519 <br /> i Client ID CPT14(93-97)11 12701 <br /> Matnx W <br /> Reporting Lima Reporting Limit <br /> Compound Concentration* Compound <br /> S Compound ConLentrahon* W S <br /> iAcetone(b) ND<15 50 25 trans-1,3-Dichioropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND to 5 0 <br /> i Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichlorometbane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoformi ND 1 0 50 Isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 1 0 50 p-lsopropyl toluene ND 10 50 <br /> i n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlorde�` ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone"I ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone ND 10 50 <br /> i• Carbon Tetrachlonde ND 10 50 Methyl tert-Butyl Ether(MTBE) - 10 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 1 0 S 0 <br /> 2-Chloroethyl Vinyl Ether`` ND 1 0 50 Styrene ND 1 0 50 <br /> Chloroform ND l 0 50 1,1,1 2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 50 1,1 2,2-Tetrachloroethane ND P50 <br /> 50 <br /> 2-Chlorotoluene ND l 0 50 Tetrachloroethene ND 50 <br /> 4-Chlorotoluene ND 10 50 Toluene ND 5 0 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 25 <br /> 1 2-Dibromo-3-chi oropropane ND 20 l0 1,2,4-Tnchlorobenzene ND 25 <br /> Dibromomethane ND 1 0 50 l,l,t-Tnehloroethane ND 50 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnchloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 50 Tnehloroethene ND 10 50 <br /> 1 4-Dichlorobenzene ND 1 0 50 Tnchlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 1 0 50 l,2,3-Tnchloropropane ND 10 50 <br /> 1 1-Dichloroethane ND 10 50 1,2,4-Trimethylbenzene 26 10 50 <br /> 1,2-Dichloroethane NO 10 50 1,3,5-Trimethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate " - ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride " ND 10 50 <br /> trans-l,2-i3ichloroethene ND 1 0 50 Xylenes,total ND 10 5 0 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 10 50- Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromotluoromethane 109 <br /> 1,1-Dichloropropene ND l 0 so Toiuene-d8 104 <br /> cis-1,3-Dichloropropene ND lo 50 4-Bromotluorobenzene 99 <br /> 'water and vapor samples are reported m ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid Sample that contains greater than--5 vol % <br /> sediment {1) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Harrulton, Lab Director <br />