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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmE22MRbellcom E-mail main@mccampbell com <br /> i <br /> Advanced GeoEnvironinental Client Project ID D I K Tracy Date Sampled 11/28/01 <br /> 837 Shaw Road Enterpnses Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br /> Client P O Date Analyzed 12/04-12/07/01 <br /> Volatile Orgamcs By GC/MS <br /> EPA method 8260 <br /> Lab ID 84528 <br /> Client ID P-15120to25 <br /> Matrix W <br /> RcpDMng Limit Rcp°mng Ltmrt <br />' Compound Concentration* W S Compound Concentration* W S <br /> Acetone(h) ND<15 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene 3 8 10 50 Ethylene dibromtde ND 10 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> aromochloromethane ND 1 0 50 Ilexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 iodomethane ND 10 50 <br /> Bromoform ND 10 50 isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND l 0 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride"' ND<2 0 1 0 50 <br /> tert-Butyl benzene ND to 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Dtsulfide ND 10 50 Methyl isobutyl ketone` ND 1 0 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlombenzene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 10 50 <br />' 2-Chloroethyl Vinyl Ether"' ND 10 50 Styrene W ND 10 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND<2 0 10 50 <br />' 4-Chlorotoluene ND 1 0 50 Toluene 28 10 50 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnehlorobenzene ND 50 25 <br /> 1 2-Dibrome-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 10 5 0 <br />' 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnehlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane ND 10 50 <br /> 1,1-Dichloroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND 10 5 0 <br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate - ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride ND 1 0 5 0 <br />' trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ° 23 10 11 <br /> 1,2-Dichloropropane ND 10 50 Comments i <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 108 <br />' 1,1-Dicbloropropene ND 10 50 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 100 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting lirmt,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than 5 Vol <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward HamuIton,Lab Director <br />