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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' 24 http l/www mccampbeIl com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID D I K Tracy Date Sampled 11/28/01 <br /> 837 Shaw Road Enterprises Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br />' Client P O Date Analyzed 12/04-12/07101 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84529 <br /> Client ID P-15/45to50 <br /> Matrix W <br /> tLepoung UME Reporting Urnit <br />' Compound Concentration* W S Compound Concentration* W S <br /> Acetone ND<15 50 25 trans-i,3-Dtchloropropene ND 10 so <br /> Benzene ND 10 5 0 Ethylene dibromide ND 10 50 <br />' Bromobenzene ND 10 5 0 Ethylbenzene ND 10 50 <br /> Bromochlorornethane ND 10 5 0 Hexachlorobutadiene ND 5 U 25 <br /> Bromodichloromethane ND 10 5 0 lodomethane ND 10 5 0 <br /> Bromoform ND 10 5 0 Isopropylbenzene ND 1 0 5 0 <br />' Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlonde�` ND<2 0 10 5 0 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl csobutyi ketone a ND 10 50 <br /> Carbon Tetrachloride ND 10 5 0 Methyl Cert-Butyl Ether(M CBE) 10 50 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 25 <br /> Chloroethane ND l 0 50 n-Propyl benzene ND 10 5 0 <br />' 2-Chloroethyl Vinyl Ether" ND 10 50 Styrene ND 1 0 50 <br /> Chloroform ND 10 50 1,1,12-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 50 t,1,2,2-Tetrachloroethane ND 1 U 50 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND<2 0 1 0 50 <br />' 4-Chlorotoluene ND 1 0 5 0 Toluene ND 10 50 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 5 0 1,1 1 Trichloroethane ND l 0 50 <br />' 1,2-Dichlorobenzene ND 10 5 0 1,1,2-Trichloroethane ND 1 10 5 0 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND l 0 50 <br /> 1,4-Dichlorobenzene ND to 50 Tnchlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 1 0 5 0 <br />' l,l-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 5 0 1 3 5-Tnmethyllienzene ND 10 5 0 <br /> 1 1-Dichloroethene ND 10 50 Vinyl Acetate `° - ND 50 25 <br /> cis-1,2-Dichioroethene ND 10 50 Vinyl Cblonde ND 10 50 <br />' <br /> trans-l,2-Dichloroethene ND 10 5 0 Xylenes,total ND 1 0 1 5 0 <br /> 1 2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2 2-Dichloropropane ND 10 1 50 1 Dmbromofluoromethane 98 <br />' l,l-Dichloropropene ND 10 1 50 1 Toluene-d8 105 <br /> cis-I 3-Dichloropropene ND LIO 1 5 0 1 4-Bmmofluorobenzene 100 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting Imus,N/A means analyte not applicable to this analysis <br /> (b) 2-proparione or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (c) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (1) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />