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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmE22MpbelI corn E-mail main@mccampbell eom <br /> i - <br /> 1 Advanced GeoEnvironmental Client Project ID D I K Tracy Date Sampled 11/28/01 <br />' <br /> 837 Shaw Road Enterprises Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tum Cuellar Date Extracted 12/04-12/07/01 <br /> Client P O Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GC/M5 <br /> EPA method 8260 <br />' Lab ID 84531 <br /> Client ID P-151 100tol05 <br /> Matrix W <br />' Compound Concentration* AW mng��miSt Compound Concentration* A- -- Ls S� <br /> Acetone cel ND<15 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene 14 10 50 Ethylene dibromide ND 1 0 5 0 <br />' Bromobenzene ND 10 50 Ethylbenzene 4 9 1 0 50 <br /> Bromochloromethane ND 10 50 Hexachlorobutadietie ND 3 0 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 50 <br /> Bromo€orm ND 1 0 50 Isopropylbenzene ND 10 50 <br />' Bromomethane ND 10 1 5 0 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 5 0 <br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chlondet` ND<2 0 10 5 0 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ND l 0 5 0 <br /> Carbon Tetrachloride ND 10 5 0 Methyl ten-Butyl Ether(MTBE) — 1 0 50 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 50 25 <br /> Chloroethane ND l 0 50 n-Propyl benzene 1 6 10 50 <br /> 2-Chloroethyl Vinyl Ether(O ND 1 0 5 0 Styrene ND 10 50 <br /> Chloroform ND 10 1 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND<2 0 10 5 0 <br /> 4-Chlorotoiuene ND 10 50 Toluene 8 0 1 0 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroethane ND 10 S D <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 1 0 5 D <br /> 1,4-Dichlorobenzene ND 10 5 0 Trichlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Trichloropropane ND 10 50 <br />' l,l-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene 13 1 0 5 D <br /> 1,2-Dichloroethane 11 to 5 0 1,3,5-Tnmethylbenzene 3 9 1 0 5 0 <br /> l,l-Dichloroethene ND 1 0 5 0 Vinyl Acetate m - ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride " ND 1 0 50 <br /> trans-l,2-Dichloroethene ND to 5 0 Xylenes,total t° 19 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> l 3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2 2-Dichloropropane ND 1 0 50 Dibromofluoromethane 109 <br /> 1,1-Dichloropropene ND l 0 50 Toluene-d8 99 <br /> cis-1,3-Dichloropropene ND t 0 5 0 4-Bromofluorobenzene 100 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> . (b) 2-propanone or dimethyl ketone, (e) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> S <br />