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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> It=//www mccam bell com E-mail main@mccampbell cum
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<br />' Advanced GeoEnvironmental Client Project ID D I K Tracy Date Sampled 11/28/01
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<br /> 837 Shaw Road Enterprises Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01
<br /> I Client P Q Date Analyzed 12104-12/07101
<br /> Volatile Organics By GC/MS
<br /> EPA method 9260
<br /> Lab ID 84530
<br /> Client ID P-15176to8l
<br /> Matrix W
<br /> Rcpomng Li mt Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* W S
<br /> Acetone(b) ND<15 50 25 trans-l,3-Dichloropropene ND 1 0 50
<br /> Benzene 6 0 10 50 Ethylene dibromide ND 1 0 50
<br /> I Bromobenzene ND 1 0 5 0 Ethylbenzene 1 2 1 0 50
<br /> Bromochloromethane ND 10 50 1-lexachlorobutadiene ND 5 0 25
<br /> Bromoaichloromethane ND 10 5 0 lodomethane ND 10 50
<br /> Bromoform ND 10 50 Isopropylbenzene ND 1 0 5 0
<br /> Bromomethane ND 10 50 p-Isopropyl toluene ND l 0 5 0
<br /> n-Butyl benzene NO 10 50 Methyl butyl ketone ND to 5 0
<br /> sec-Butyl benzene ND 10 50 Methylene Chloride` ND<2 0 10 50
<br /> tert-Butyl benzene ND 1 0 5 0 'Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone ND 10 50
<br /> Carbon Tetrachloride ND 10 5 0 Methyl tert-Butyl Ether(MTBE) 1 0 5 0
<br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 25
<br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 1 0 5 0
<br /> 2-Chloroethyl Vinyl Effiet" ND 10 50 Styrene ND 1 0 5 0
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50
<br /> 2-Chlorotoluene ND l 0 50 Tetrachloroethenc NDK2 0 1 0 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 37 10 5 0
<br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1 2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnehlorobenzene ND 5 0 25
<br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 50
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 1 0 50
<br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 5 0
<br /> 1 4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 5 0
<br /> Dichlorodifluoromethane ND 10 50 12,3-Tnchloropropane ND 10 50
<br /> 1 i-Dichloroethane ND 10 50 1,2,4-Tnrnethylbenzene 20 10 50
<br /> 1,2-Dichloroethane ND 10 50 1,3,5-Trimethylbenzene ND 10 50
<br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate "' - ND 50 25
<br /> cis-1,2-Dichloroethene ND 10 1 5 0 Vinyl Chloride ND 10 5 0
<br /> trans-l,2-Dichloroethene ND 10 50 Xylenes,total 4 5 1 0 50
<br /> 1,2-Dichloropropane ND 10 5 0 Comments 1
<br /> 1,3-Dicbloropropane ND to 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 5 0 Dibromofluoromethane III
<br /> 1,1-Dichloropropene ND 10 5 0 Toluene-dS 104
<br /> cis-1,3-Dichloropropane ND 10 50 4-137`011710fluorobenzene 100
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> I ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2-
<br /> pentanone or tsopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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