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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 14 htto//www mccamubellcom E-mail main@mccampbell cam <br /> Advanced GeoEnvtronmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/04-12/07/01 <br /> Client P Q Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 84503 <br /> Client ID P16(15-20)/112901 <br /> Matnx W <br /> Compound Concentration* itepor Lim t Compound Concentration* Rcporhng Lunn <br /> W S W S <br /> Acetone lel ND 50 25 trans-1,3-Dichloropropene ND 1 0 5 0 <br /> Benzene 130 10 5 0 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 10 50 Ethylbenzene 73 10 5 0 <br /> Bromochioromethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 5 0 lodomethane ND to 50 <br /> Bromotorm ND 10 5 0 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone` ) ND 10 50 <br /> sec-Butyl benzene ND 10 5 0 Methylene Chlonde e' ND 1 0 i 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone' ND 2 0 l0 <br /> lieCarbon Disulfide ND 1 0 5 0 Methyl isobutyl ketones ND 10 5 0 <br /> Carbon Tetrachlonde ND 1 0 50 Methyl tort-Butyl$cher(MTBE) 10 5 0 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND to –7-0 <br /> 2-Chloroethvl Vmyi Ether" ND 1 0 50 Styrene ND ] 0 50 <br /> Chlorotorm ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 10 5 0 <br /> 4-Chlarotoluene ND 10 5 0 Toluene U1 10 1-0 5 0 <br /> DibromochIoromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chi oropropane ND 2 0 10 42,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnehloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnehloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Tnchloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Tnchlorofluoromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 1 1 0 5 0 <br /> 1,1-Dichloroethane ND l 0 5 0 1,2,4-Trimethylbenzene 11 1 0 5 0 <br /> 1 2-Dtchloroethane 6 7 10 5 0 1,3,5-Trtmethylbenzene ND 1 0 '50 <br /> l,l-Dichloreethene ND 10 50 Vinyl Acetate ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chlonde " ND l 0 5 0 <br /> I trans-1,2-Dichioroethene ND 10 5 0 Xylenes,total 14 1 0 =0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 TOβ€” Dibromofluoromethane 108 <br /> 1 l-Dichloropropene ND 10 5 0 Toluene-dg 105 <br /> cis-1,3-Dichloropropene ND 1 D 5 0 4-Bromofluorobenzene 99 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting knit,N/A means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscibie sheen is present, (t) liquid sarnple that contains greater than –5 vol % <br /> sediment, 0) sample diluted due to high organic Lontent, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> Lhloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />