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p 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ® McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccMRbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmentaI Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br />' Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br /> Client P O Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84504 <br /> Client ID P16(36-40)/7 12901 <br /> Matrix W <br /> Repo- <br /> ng Limit Reporting Limit <br />' Compound Concentration* W S Compound Concentration* <br /> W S <br /> Acetone n} ND<10 5 0 25 trans-1,3-Dichloropropene ND 1 0 5 0 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50 <br />' Bromobenzene ND 1 0 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND c 0 25 <br /> Bromodichloromethane ND 1 0 50 ]odomethane ND 1 0 1 50 <br /> Bromoform ND 1 0 50 lsopropy[benzene ND 10 50 <br />' Bromomethane ND 1 0 50 p-Isopropyl toluene ND i 0 1 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 �0 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride" ND<5 0 10 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 to <br /> Carbon Disuihde s ND 1 0 50 Methyl isobutyl ketone g' ND 1 0 so <br /> Carbon Tetrachloride ND l 0 50 Methyl tett-Butyl Ether(MTBE) — 1 0 50 <br /> Chlorobenzene ND l 0 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 10 50 <br /> 2-Chloroethyl Vinyl Ether` ND L 0 50 Styrene ND I 0 1 5 0 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chiorotoluene ND 1 0 50 Tetrachloroethene ND 10 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 10 50 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchloroberizene ND 30 25 <br /> 1 2-Dibromo-3-chloropropane ND 20 10 1 2 4-Tnchlorobenzene ND 50 ZS <br /> Dibromomethane ND 1 0 50 1,1 1-Trichloroethane ND 1 0 50 <br /> t 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Tnehloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnehlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 1 0 50 1 2 3-Tnchloropropane ND 10 50 <br /> 1,1-Dichloroethane ND 10 50 1,2 4-Trimethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 1 3,5-Tnmethylbenzene ND to 5 0 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate m ND 50 25 <br /> tis-1,2-Dichioroethene ND 10 so Vinyl Chloride ND 10 50 <br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes total ° ND 1 0 50 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND to 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 5 0 Dibromotlucromethane �L97l,l-Dichloropropene ND 1 0 5 0 Toluene-d8 cis-1,3-Dichloropropene ND 1 0 5 0 4-Bromotluorobenzenc <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene ) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />