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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www_mccampbell corn E-mail matn@a mccampbell corn <br />' Advanced GeoEiivuonmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br />' 837 Shaw Road <br /> Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12104-12/07/01 <br /> I Client P O Date Analyzed 12/04-12/07/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84508 <br /> Client ID P17(18-22)/112901 <br /> Matrix W <br /> Rcpomng Limit Repomng Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone(b) ND<60 50 25 trans-l,3-Dichlorapnopene ND<S 0 10 50 <br /> Benzene 28 10 50 Ethylene dibromide ND<50 1 0 5 0 <br /> Bromobenzene ND<5 0 1 0 50 Ethylbenzene 1 24 10 5 0 <br /> Bromochloromethane ND<5 0 10 1 50 Hexachlorobutadiene ND<25 5 0 25 <br /> Bromodicnloromethane ND<5 0 1 0 1 5 0 lodomethane ND<5 0 1 0 50 <br /> Bromotorm ND<5 0 1 0 , S 0 Isopropylbenzene NIKS 0 10 50 <br />' Bromomethane ND<5 0 1 0 5 0 p-Isopropyl toluene ND<5 0 10 50 <br /> n-Butyl benzene ND<5 0 10 5 0 Methyl butyl ketone' ND<5 0 10 �0 <br /> see-Butyl benzene ND<5 0 1 0 5 0 Methylene Chlande° ND<10 10 5 0 <br /> tert-Butyl benzene ND<5 0 1 0 5 0 Methyl ethyl ketone ND<10 2 0 10 <br /> Carbon Disulfide ND<5 0 to 5 0 Methyl isobutyl ketone ix ND<5 0 1 0 5 0 <br /> Carbon Tetrac litondc. ND<5 0 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Chlombenzene ND<5 0 1 0 50 Naphthalene ND<25 50 25 <br /> Chloroethane ND<5 0 1 0 5 0 n-Propyl benzene 55 l 0 50 <br /> 2-Chloroethyi Vinyl Ethe ND<5 0 1 0 5 0 Styrene 11 ND<5 0 1 0 5 0 <br /> Chlorotorm ND<5 0 1 0 50 l,] 1,2-Tetrachlor(3ethane ND<5 0 1 0 5 0 <br /> Chloromethane ND<5 0 1 0 50 1,1,2,2-Tetrachloroethane ND<50 1 0 50 <br /> 2-Chlorotoluene ND<5 0 1 0 50 Tetrachloroethene ND<5 0 10 50 <br /> 4-Chlorotoluene ND<5 0 1 0 5 0 Toluene 14 1 0 5 0 <br /> Dibromochloromethane ND<5 0 1 0 50 1,2,3-Tni,hiorobenzene ND<25 50 25 <br /> 1,2-Dibromo-3-chloropropanc ND<10 2 0 10 1 2,4-Tnchlorobenzene ND<25 5 0 25 <br /> Dibromomethane ND<5 0 1 0 50 1,1,1-Trichloroethane ND<5 0 1 0 5 0 <br /> 1,2-Dichlorobenzene ND<5 0 1 0 5 0 1,1,2-TnLhloroethane ND<5 0 1 0 50 <br /> 1,3-Dichlorobenzene ND<5 0 l 0 50 Trichloroethene ND<5 0 1 0 5 0 <br /> 1,4-Dichlorobenzene ND<5 0 1 0 5 0 Tnehlorofluoromethane ND<5 0 10 50 <br /> Dichlorodifluoromethane ND<5 0 1 0 5 0 1,2,3-Tnchloropropane ND<5 0 10 5 0 <br /> 1 l-Dichloroethane ND<5 0 1 0 5 0 1,2,4-Tnmethylbenzene 45 10 -,)0 <br /> 1,2-Dtchloroethane ND<5 0 10 5 0 1,3,5-Tnmethylbenzene 10 ] 0 S Q <br /> 1,1-Dichloroethene ND<5 0 10 50 Vinyl Acetate 'IND<25 50 25 <br /> cis-1,2-Dichloroethene ND<5 0 1 0 5 0 Vinyl Chloride " ND<5 0 1 0 5 0 <br /> trans-1,2-Dichloroethene ND<5 0 1 0 5 0 xylenes,total i° 95 1 0 0 0 <br /> 12-Dichloropropane ND<5 0 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND<5 0 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-❑ichloropropane ND<5 0 1 0 5 0 Dibromotluoromethane 101 <br /> 1,1-Dichloropropene ND<5 0 1 0 so Toluene-d8 97 <br /> cis-1,3-Dichloropropene ND<5 0 l 0 5 0 4-Bromotluorobenzene 94 <br /> water and vapor samples are reported in ug/L soil and sludge samples in ug/kg,wipes m ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting]mut,N/A means analyte not applicable to this analysis <br /> • (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (t) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />