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110 2nd avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 � <br /> http//www mccamnbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID D I K Tracy Ent Date Sampled 11/29/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01 <br /> Client P 0 Date Analyzed 12104-12/07/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> I Lab ID 84509 <br /> Client ID P17(42-46)/112901 <br /> Matrix W <br /> Reporting Limit Repomng Limit <br /> I Compound Concentration* W 9 Compound Concentration* w S <br /> Acetone t" 14D<15 50 , 25 trans-1,3-Dichioropropene ND 1 0 50 <br /> Benzene ND 10 50 Ethylene dibromrde ND 1 0 50 <br /> Bromobenzene ND 10 50 Ethylbenzene 1 14 1 0 50 <br /> Bromochloromethane ND 10 50 Hexachlombutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND l 0 5 0 <br /> Bromotorm ND 10 50 Isopropvlbenzene ND 1 0 50 <br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone`6} ND 1 0 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride'' -7. ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone'91 ND 1 0 :0 <br /> lie Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene ND 10 50 Naphthatene ND 5 0 25 <br /> Chloroethane ND l 0 50 n-Propyl benzene ND 1 0 50 <br /> I 2-Cbloroethyl Vinyl Ether" ND 1 0 5 0 Styrene ND 1 0 50 <br /> Chloroform ND l 0 50 1,1,1,2-Tetrachloroethane ND 1 0 a D <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND I 0 50 <br /> 2-Chiorotoluene ND 10 50 Tetrachloroethene ND I 0 5 0 <br /> I 4-Chiorotoluene ND 1 0 50 Toluene` ND 1 0 50 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1 2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1 1,1-TnchloroethanL ND 1 0 50 <br />' 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 1 0 50 <br /> l 3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Trichloropropane ND 1 0 50 <br /> l,l-Dichloroethane ND 10 50 12,4-Tnmethylbenzene 16 l0 50 <br /> 1,2-Dichloroethane ND 10 so 1,3 5-Tnmethylbenzene _ ND 1 0 50 <br /> 1,1-Dichloroethene ND 1 0 50 Vinyl Acetate 01 ND 50 25 <br /> I cis-1,2-Dichioroethene VD 10 50 Vinyl Chloride °' ND 1 0 50 <br /> trans-l,2-Diehloroethene ND 10 50 Xylenes,total 45 1 0 50 <br /> 1 2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 107 <br /> l,l-Dichloropropene ND 1 0 5 D Toluene-i8 95 <br /> c.1s-1,3-Dichioropropene ND LLO L5O 4-Bromefluorobenzene Ill <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> . (b) 2-propanone or dimethvl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hecanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyi-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (t)liquid sample that contains greater than --5 voi % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> oro <br /> chlethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />