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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> MCCA IPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www rn=pbell cum E-mail main@mccampbell corn
<br /> Advanced GeoEnvironmental Client Project ID D F K Trac Ent Date Sampled 11/29/01
<br /> J Y
<br /> 837 Shaw Road Date Received 11/30/01
<br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/04-12/07/01
<br /> Client P O Date Analyzed 12/04-12/07/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> I Lab ID 84510
<br /> Client ID P17(76-80)1112901
<br /> Matrix W
<br /> itepomng Limit Reporting Limit
<br /> Compound Concentration* W S Compound Concentration* � W S
<br /> acetone ch) ND<I� T05
<br /> trans-4,3-Dichloropropene NO to 50
<br /> Benzene i t Ethylene dibromide NO 10 50
<br /> Bromobenzene ND Ethylbenzene 12 1 0 50
<br /> Bromochloromethane 1,113 Hexac.hlorobutadiene ND 50 25
<br /> Bromodtchloromethane ND lodomethane ND 10 5 0
<br /> Bromworm ND Isopropylbenzene 1 8 10 5 0
<br /> Bromornethane ND l 0 50 p-Isopropyl toluene NO 10 5 0
<br /> n-Butyl benzene 34 1 0 5 0 Methyl butyl ketone` ' ND 10 so
<br /> sec-Butyi benzene l 0 10 50 Methylene Chloride(` ND<2 0 No 50
<br /> teri-Butyl benzene NO 10 50 btethyl ethvl ketone( ND 10
<br /> Carbon Disulfide NO 1 0 50 Methyl isobutyl ketone e NO 50
<br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butvl Ether(MTBE) 50
<br /> Cnlorobenzene NO 10 50 Naphthalene ND 25
<br /> Chloroethane ND 1 0 50 n-Propyl benzene 60 50
<br /> '-Chloroethyl Vinyl Ether(c) ND to 50 Styrene( NO 1 0 50
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane NO 1 0 5 0
<br /> Chloromethane ND 10 50 1 1 2 2-Tetrachloroethane NO 10 50
<br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 10 50
<br /> 4-Chlorotoluene ND 10 50 Toluene 62 10 50
<br /> Dibrumochloromethane ND 1 0 50 1 2,3-Tnchlorobenzene ND 50 25
<br /> 1,2-Dibromo-3-chloropropane NO 20 to 12,4-Tnchlorobenzene NO 50 25
<br /> Dibromamethane ND 10 10 1,1,1-Trichloroethane NO 10 111
<br /> 1 2-Dichlorobenzene. NO to 50 1,1,2-Trichloroethane ND 1 0 50
<br /> 1,3-Dichlorobenzene ND to 50 Tnchloroethene ND 1 0 50
<br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane NO 10 50
<br /> Dichlorodifluoromethane NO 10 50 1,2,3-Tnchloropropane ND 10 5 0
<br /> I,I-Dtchloroethane ND 10 50 1,2,4-Tnmethylbenzene 37 1 0 50
<br /> 1,2-DichloroethanL ND 10 50 1,3,5-Trimethylbenzene NO 10 50
<br /> l,l-Dichloroethene ND 10 50 Vinyl Acetate ND 50 25
<br /> I cis-i,2-Dtchloroethene ND 10 50 Vinyl Chloride(n) NO 10 50
<br /> trans-1 2-Dtchloroethene NO 10 50 Xylenes,total 43 ] 0 5 0
<br /> 1,2-Dtchloropropane NO 10 50 Comments
<br /> 1,3-Dcchloropropane ND 10 50 Surrogate Recoveries(%)
<br /> 2,2-Dcchloropropane NO 10 5 D Dibromofluoromethane 105
<br /> l,l-Dtchloropropene ND 10 50 1 Toluene-dg 95
<br /> c.is-1,3-Dtchloropropene NO 1 0 5 0 IJ 4-Bromofluorobenzene III
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysts
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (t) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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