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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> 4 MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> //www_mccampbell com E-mail main@mccampbell com
<br /> Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/30/01
<br /> 837 Shaw Road Date Received 12/04/01
<br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/07-12/11/01
<br /> Client P O Date Analyzed 12/07-12/11/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 84745
<br /> Client ID P17(91-96)/113001
<br /> Matrix W
<br /> Reporting Limit Reporting Limit
<br /> Compound Concentration* Compound S Compound Concentration* W 3
<br /> Acetone W ND<10 50 1 25 trans-1,3-Dichloropropene ND 1 0 so
<br /> Benzene 2 7 10 50 Ethylene dibromide ND 1 0 5 0
<br /> Bromobenzene ND 10 50 Ethylbenzene 1 7 1 0 50
<br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 10 5 0 Iodomethane ND 1 0 50
<br /> Bromoform ND 10 5 0 lsopropylbenzene ND 1 0 50
<br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 50
<br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 1 0 50
<br /> sec-Butyl benzene ND 10 5 0 Methylene Chlorides` ND<2 0 1 0 5 0
<br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ND 1 0 50
<br /> Carbon Tetrachloride ND 1 0 5o Methyl tert-Butyl Ether(MTBE) 1 0 5 0
<br /> Chlorobenzene ND 1 0 50 Naphthalene 94 5 0 25
<br /> Chloroethane ND to 5 0 n-Propyl benzene ND 1 0 5 0
<br /> 2-Chloroethyt Vinyl Ether(`) ND 10 50 Styrene MND 1 0 5 0
<br /> Chloroform ND l 0 50 1,1,1,2-Tetrachloroethane ND 1 0 5 0
<br /> Chloromethane ND l 0 5 0 1 12,2-Tetrachloroethane ND 1 0 5 0
<br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 1 0p5o
<br /> I 4-Chiorotoluene ND 1 0 50 Toluene 1 6 1 0
<br /> Dtbromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnehlorobenzene ND 5 0
<br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 1 0
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10
<br /> 1,3-1)icblorobenzene ND 10 5 0 Trichloroethene ND 1 0 5 0
<br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 5 0
<br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnehloropropane ND 1 0 5 0
<br /> 1,1-Dichloroethane ND to 5 0 1,2,4-Tnmethylbenzene 4 0 1 0 5 0
<br /> 1,2-Dichloroethane ND to 5 0 1,3,5-Tnmethy1benzene ND 1 0 5 0
<br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate em - ND 5 0 25
<br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride iu ND 1 0 LO -
<br /> trans-
<br /> l,2-Dichloroethene ND 1 0 5 0 Xylenes,total 65 1 0
<br /> 1,2-Dichloropropane ND 10 5 0 Comments
<br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane ]01
<br /> 1,1-Dichloroproperie ND 1 0 5 0 Toluene-d8 98
<br /> cis-1,3-Dichloropropene ND 10 50 4-Bromotluorobenzene 94
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> Nb means not detected above the reporung limit N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (t) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or tsopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample, that contains greater than --5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 9) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene (o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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