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I <br /> I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAIMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@mccampbell corn <br />' Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/30/01 <br /> 837 Shaw Road Date Received 12/04/01 <br />' Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/07-12/11/01 <br />' Client P O Date Analyzed 12/07-12/11/0 1 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 84746 <br /> Client ID P17(117-120)/113001 <br /> Matnx W <br /> Repomng Lirmi Reporting Unit <br /> Compound Concentration* Compound Concentration* <br /> WI S W S <br /> Acetone cb> ND<10 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene 1 8 1 0 50 Ethylene dibromide ND to 50 <br />' Bromobenzene ND 10 50 Ethylbenzene 3 0 10 50 <br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 10 5 0 lodomethane ND 10 1 5 0 <br /> Bromotoim ND to 50 Isopropylbenzene ND 1 0 5 0 <br />' Bromomethane ND 1 0 50 p4sopropyl toluene ND to 5 0 <br /> n-Butyl benzene 1 2 1 0 50 Methyl butyl ketone ND to —50 <br /> sec.-Butyl benzene ND 1 0 50 Methylene Chlondet° ND<2 0 10 5 0 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone M ND 2 0 10 <br />'• Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone 4 ND 1 0 5 0 <br /> Carbon Tetrachloride SID 10 50 Methyl tert-Butyl Ether(MI BE) 1 0 5 0 <br /> Chlorobenzene ND 10 5 0 Naphthalene 15 5 0 25 <br /> Chloroethane ND 10 5 0 n-Propyl benzene 1 3 10 50 <br /> 2-Chloroethyl Vinyl Htherc`' ND 1 0 50 Styrene` ND 40 5 0 <br /> Chloroform ND 1 0 50 l,l 1,2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND l 0 50 Tetrachloroethene ND 1 0 5 0 <br /> a-Chlorotoluene ND 1 0 50 Toluene 1 7 1 1 0 50 <br /> Dtbromochloromethane ND 10 5 0 1,2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25 <br /> Dibromomethane ND 1 D 1 50 1,1,1-Trichloroethane ND I O 5 D <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchloroftuoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnehloropropane ND 10 5 0 <br />' 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene 10 10 50 <br /> 42-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene 2 l FTO 5 0 <br /> I,1-Diehloroethene ND 1 0 5 0 Vinyl Acetate m ND5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride " ND 1 0 5 0 <br /> trans-l,2-Dichloroelhene ND 10 5 0 Xylenes,total ° 12 1 0 50 <br /> 1,2-Dichloropropane ND 1 0 50 Comments h <br /> 1 3-Dichloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2 2-Dichloropropane ND 10 50 Dibromolluoromethane 101 <br /> I,I-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene {o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />