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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' McCAINUBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> . http//www mccampbell co m E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Protect 1D Three B's Date Sampled 11/30/01 <br />' 837 Shaw Road Date Received 12/04/01 <br /> Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br />' Client P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> =.ethod264 <br /> Lab ID 84751 <br /> Client ID P18(114-118)/113001 <br /> Matrix W <br /> Compound Concentration* Rwmng Lit IF Compound Concentration.* Rcpornng L:St <br /> Acetone ins ND<10 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND ] 0 50 Ethylene dibromide ND 1 0 50 <br /> Bromobenzcne ND to 50 Ethyibenzene ND 1 0 50 <br /> Bromochloromethane ND 1 0 50 1-iexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoform ND 1 0 50 lsopropy[benzene ND 10 1 50 <br />' Bromomethane ND 10 50 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND to 50 Methyiene Chlonde ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 20 14 <br /> Carbon Disulfide ND 1 0 50 Methyi isobutyl ketone is ND 1 0 50 <br /> lie Carbon Tetrachionde ND 1 0 50 Methyl tert-Butyl Ether(M ME) 1 0 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 25 <br /> Chloroethane ND 1 0 50 n-Propyl benzene ND 1 0 so <br /> 2 Chloroethyl Vinyl Ether() ND 10 50 Styrene ND 1 0 5 0 <br /> Chloroform ND 10 50 1,1,1,2-tetrachloroethane ND l0 50 <br /> Chloromethane ND l0 50 1,1,2,2-Tetrachioroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 50 retrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 1 0 50 <br /> Dibromochloromethane ND 1 0 50 1,2,3-Tnchiorobenzene ND 1 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Trichloroethane ND 1 0 �0 <br /> 1,2-Dichicrobenzene ND 10 50 1 1,2-Trichloroethane ND 1 0 50 <br /> 1,3-Dichiorobenzene ND 1 0 50 Tnchioroethene ND 1 0 50 <br /> 1 4-Dichlorobenzene ND 1 0 50 Tnchiorotluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane ND 1 0 50 <br /> M-Dichloroethane ND 1 0 50 1,2,4-Tnmethylbenzene ND 1 0 50 <br /> i,2-Dichloroethane ND 1 0 50 1,3,5-Tnmethylbenzene ND 1 0 50 <br /> 1,1-Dichloroethe-re ND 1 0 50 Vinyl Acetate " ND 50 25 <br /> c,is-1,2-13ichloroethene ND 1 0 5 0 Vinyl Chloride ° ND1 0 L5O <br /> trans-l,2-Drchloroethene ND 1 0 50 Xylenes,total ND 1 0L <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dtchloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> I 2,2-Dtchloropropane ND 1 0 50 Dibromotluoromethane 103 <br /> i,l-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> I ND means not detected above the reporting limit,N/A means analyte not apphcable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or rsopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> ehloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />