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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br />' MCCAIMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-16222 <br /> 14 http/lwww mcc bcll com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID 'Three B's Date Sampled 11/30/01 <br />' $37 Shaw Road Date Received 12/04/01 <br /> Stockton,CA 95215 CIient Contact Tun Cuellar Date Extracted 12/07-12/11/01 <br />' Client P O Date Analyzed 12/07-12/11/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8264 <br />' Lab ED 84750 <br /> Client ED P18(99-103)/113001 <br /> Matrix W <br /> ICompound Concentration* x :g L'Si Compound Concentration* tt W ng Limi <br /> Acetone cel ND<10 50 25 trans-1,3-Dichloropropene ND I 0 50 <br /> Benzene ND 1 0 50 Ethylene dibromtde ND 1 0 50 <br /> Bromobenzene ND 1 0 5 0 Ethyibenzene ND 1 0 5 0 <br /> Bromochloromethane ND 1 0 50 13exachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND I 0 50 Iodomethane ND 10 5 0 <br /> Bromoform ND I 0 50 Isopmpylbenzene ND 1 1 0 5 0 <br /> Bromomethaue ND 10 50 p-isopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene ND To 5 0 Methyl butyl ketone ND 1 0 5 0 <br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride"' NIK2 0 1 0 50 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone i ND 2 0 10 <br /> Carbon Disulfide ND 1 0 5 0 Metbyl isobutyl ketones ND 1 0 50 <br /> lie Carbon Tetrachloride ND 1 0 50 Methyl tent-Butyl Ether(MTBE) l 0 50 <br /> Chlorobenzene ND 1 0 5 0 Naphthaiene ND 5 0 25 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether" ND 1 0 50 Styrene MND 1 6 50 <br /> Chloroform ND 1 0 5 0 1 1 1,2-Tetrachloroethane ND 10 50 i <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotaluene ND 1 0 5 0 Tetrachioroethene ND 1 0 5 0 <br /> I 4-Chlorotoiuene ND 1 0 5 0 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnc,hiorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3�hloropropane ND 2 0 10 1 2,4-Tnchlorobenzene ND 5 0 25 <br /> I Dibromomethane ND 1 0 5 0 1 I,i-Trichloroethane ND 1 0 5 0 <br /> 1 2-Dichlorobenzene ND 10 5 0 1 1,2-Tnchloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 10 5 0 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 1 0 so <br /> Dichlorodtfluoromethane ND 1 0 5 0 1 2,3-Trichloropropane ND 10 5 0 <br /> LI-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 1 0 5 0 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate m ND 50 25 <br /> I cis-1 2-Dichloroethene ND l 0 5 0 Vinyl Chloride`° ND 1 0 5 0 <br /> trans-1 2-Dichloroethene ND 1 0 5 0 Xylenes,total i° ND 1 0 S b <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries(%) <br /> I 2,2-Dichloropropane ND 10 50 Dibromotluoromethane 103 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 98 <br /> cis-1,3-Dichloropropene ND 10 50 4-Brornotluorobenzene 94 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L. <br /> ND means not detected above the reporting hrrut,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methvl-2 <br /> pentanone or isopropylacetone, (h) lights than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, (1) sample diluted due to high organic content, (k) ethenylbenzene, methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chioroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> I <br />