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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br />' 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> h9EL/www mccampbell com E-mail main@mccampbell com
<br /> Advanced GeoEnvironinental Client Project ID Three B's Date Sampled 11/26-11/27/01
<br /> 837 Shaw Road Date Received 11/30/01
<br /> EStockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01
<br /> Client P O Date Analyzed 12103-12/06101
<br /> I
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 84511
<br /> Client ID CPT13(16-20)1112601
<br /> Matrix W
<br /> Compound Concentration* Reporting Limit Compound Concentration* Rcpomng Limit
<br /> w S W 5
<br /> Acetone id ND<15 50 25 trans-I 3-Dichloropropene ND 1 0 50
<br /> Benzene ND t 0 50 Ethylene dibromide ND 1 0 50
<br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 10 50
<br /> Brornochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 2:
<br /> Bromodichloromethane ND 10 5 0 Iodomethane ND 10 5 0
<br /> Broinofortn ND 10 50 Isopropylbenzene ND 1 0 50
<br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 1 0 5 0
<br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 1 0 50
<br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND<2 0 10 50
<br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 20 10
<br /> Carbon Disulfde ND 10 50 Methyl isobutyl ketone ND 1 0 5 0
<br /> Carbon Tetrachloride ND 1 0 5 0 Methyl ten-Butyl Ether(MTBE) 1 0 50
<br /> Chlombenzene ND 10 50 Naphthalene ND 50 25
<br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 0 50
<br /> 2-Chloroethyl Vinyl Ethe ND 10 5 0 Styrene ND 1 0 50
<br /> ChIorotorm ND 1 0 1. 5 0 1,1,12-Tetrachloroethane ND 1 0 5 0
<br /> Chloromethane ND 10 50 1,1,2 2-Tetrachloroethane ; SID 10 50
<br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 10 50
<br /> 4-Chlorotoluene ND 10 50 Toluene ND 1 0 5 0
<br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropme ND 20 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 10 50 1,1,2-Tnchloroethane ND 1 0 5 0
<br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND 10 50 Tnchloroethene ND 10 50
<br /> 1,4-Dichlorobenzene ND 10 50 Tnchlorofluaromethane ND 10 50
<br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropmpane ND 10 50
<br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 10 50
<br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethyibenzene ND 10 50
<br /> I,1-Dichloroethene ND 10 50 Vinyl Acetate °' _ ND 5 0 25
<br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chlonde " ND 1 0 50
<br /> trans-l,2-Dichlomethene ND 10 5 0 Xylenes,total ND 10 5 0
<br /> 1,2-Dichloropropane ND 10 5 0 Comments
<br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 87
<br /> 1 1-Dichloropropene ND 1 0 5 0 Toluene-d8 117
<br /> cis-1,3-Dichtoroproperic ND 1 0 5 0 4-$romofluorobenzene l00
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPI-P extracts in ug/L
<br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroetboxy) ethene, (d) 2-hexanone, (e) dichloromethane, (0 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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