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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccampbell com E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O Date Analyzed. 12/03-12/06/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 0 84512 <br /> Client ID CPT13(38-42)/112601 <br /> Matrix W <br /> Rcpaung Limit Reporting Limit <br /> Compound Concentration* W 3 Compound Concentration* Reporting <br /> S <br /> Acetone cb ND<15 50 25 trans-1,3-Dich1oropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dlbromrde ND 10 50 <br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 1 0 j :)0 <br /> Bromochloromethane ND 10 50 Hexachlorubutadiene ND 5 0 1 25 <br /> Bromodichlorornethane ND 1 0 50 lodomethane ND 1 0 5 0 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND to 5 0 <br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride"' ND<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone` ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone ND 1 0 5 0 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) --- 1 0 5 0 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene ND 5 0 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 0 5 0 <br /> 2-Chloroethyl Vinyl Ether" ND 1 0 5 0 Styrene ND 10 5 0 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 10 5o 11 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 10 50 1,2,3-Tnchlorobenzene ND 50 25 <br /> 1,2-13ibromo-3-chloropropane ND 2 0 10 1,2,4-Tnehlombenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnehloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND l 0 50 Tnchloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND to 50 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnehloropropane ND 10 50 <br /> 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1 2-Dichloroethane ND 10 5 0 1 3,5-Trimethylbenzene ND to 5 0 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate _ ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ° ND 10 5 0 <br /> I trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 10 1 5 0 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluotemethane 115 <br /> I <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 123 <br /> cis-1,3-Dichloropropene ND 10 5 0 4-B1amofluorobenzene 99 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/unpe and all TCLP/SPLP extracts in ug/L <br /> I ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, {1) sample diluted due to high organic content (k) ethenylbenzene, 1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />