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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h"//www mccampbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironrnental Cheat Project ID Three B's <br /> Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O Date Analyzed 12103-12/06/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 84515 <br /> Client ID CPT13(136-140)/112601 <br /> Matrix W <br /> kcporting Limst Rtyiorttng L=tCompound Concentration* W S Compound Concentration* ep S <br /> Acetone iai ND<15 5 0 25 trans-l,3-Dichloropropene ND 1 0 5 0 <br /> Benzene ND 1 0 50 Ethylene dibromide ND —1-0- 50 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 10 5 0 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 ::5:0: <br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 1 0 5 0 <br /> E Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND —10 5 0 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND l 0 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chlonde" ND<2 0 1 0 5 0 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10 <br /> lieCarbon Disulfide ND to 5 0 Methyl isobutyl ketones ND 1 0 5 0 <br /> Carbon Te=chlonde ND 10 5 0 Methyl tert-Butyl Ether(MTBE) 1 0 5 0 <br /> Chlorobenzcne ND to 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 0 50 <br /> 2-Chlomethyl Vinyl Ether` ND 1 0 5 0 Styrene ND 1 0 5 0 <br /> Chloroform ND 10 50 1,1 1,2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND l 0 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachioroethene ND 1 0 50 <br /> 4-Chiorotoluene ND 10 50 Toluene ND 1 0 5 0 <br /> Dibromochioromethane ND 10 50 1,2 3-Tnchiorobenzene ND 5 0 25 <br /> 1,2-Dibrotno-3-chlorupropane ND 20 10 1,2,4-Tnchlorobenzme ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Tncbloroethane ND 10 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 50 t,l 2-Tnchloroethane ND 1 0 5 0 <br /> 1,3-Dichlorobenzene ND 10 50 Tnchioroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 1 0 50 <br /> 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 1 0 50 <br /> 1,2-Dichicroethane ND 10 50 1 3,5-Tnmethylbenzene ND 1 0 50 <br /> l,l-Dichloroethene ND 1 0 50 Vinyl Acetate `9 - ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ND 10 50 <br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 10 5 0 <br /> 1,2-Dichloropropane ND 10 1 50 Comments <br /> 1,3-Dichloropropane ND 1 0 5 D Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromofluoromethane 119 <br /> 1,1-Dichloropropene ND to 5 0 Toluene-d8 94 <br /> cis-1,3-Dichioropropene ND 10 50 4-Bromofluorobenzene 100 <br /> water and vapor samples are reported m ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting hmit,N/A means analyte ,,,,,applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (t) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water initmscib€e sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> E chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />