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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br />' WCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mecamvbell-com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental CIient Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> Client P O I Date Analyzed 12103-12/06/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84514 <br /> Client ID CPT13(96-100)/112601 <br /> Matrix W <br /> Reponmg L[m[t Repomng Limit <br />' Compound Concentration* W S Compound Concentration* ep S <br /> Acetone(b) ND<15 5 0 25 trans-1,3-Dichloropropene ND r5(0) <br /> 50 <br /> Benzene ND ]0 5 0 Fthylene dibromide ND 5 0 <br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 5 0 <br /> Bromochloromethane ND 1 0 5 0 Hecachlorobutadiene ND 25Bromodichloromethane ND 1 0 5 0 lodomethane ND 5 0Hramotorm ND 1 0 5 0 Isopropylbenzene ND 5 0 <br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ' ND 1 0 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chlonde° ND<2 0 10 50 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 1 0 5 0 Methyl isobutyl ketone'g' ND 1 0 5 0 <br /> Carbon Tetrachlonde ND 10 5 0 Methyl tent-Butyl Ether(MTBE) 1 0 5 0 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND 10 50 n-Propyl benzene ND 10 5 0 <br /> 2-Chloroethyl Vinyl Ether` ND 1 0 5 0 [1,1 <br /> tyrene ND 10 5 0 <br /> Chloroform ND 1 0 50 ,1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 1 0 5 0 2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 etrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 5 0 oluene ND 10 5 0 <br /> Dibromochioromethane ND 1 0 5 0 1,2,3-Tnchloroben7ene ND 5 0 25 <br /> 1,2-Dibrorno-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzene ND 5 0 25 <br /> Dibromomethane ND 10 50 1,1,1-Trichloroethane ND 10 50 <br /> 12-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND l0 50 <br /> 1,3-Dichlorobenzene ND l 0 50 Trichloroethene ND 1 0 5 0 <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND l 0 5 0 1,2,3-Tnehloropropane ND l 0 50 <br /> 1,1-Dichioroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene ND l 0 5 0 <br /> 1,2-Dtchloroethane ND 10 5 0 1,3 5-Tnmethylbenzene ND 10 5 0 <br /> ],1-Dichloroethene ND 1 0 5 0 Vinyl Acetate im - ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride " ND 10 5 0 <br /> trans-1,2-Dichloroethene ND l 0 50 Xylenes,total ND 1 4 5 0 <br /> 1,2-Dichloropropane ND l 0 50 Comments <br /> 1,3-Dichloropropane ND t 0 50 Surrogate Recoveries <br /> 2,2-Dichloropropane ND 1 0 50 Dibromotluoromethane 116 <br /> I 1,1-Dichloropropene ND 1 0 50 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 1 0 5 0 4-13romofluorobenzene 99 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> I ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (t) 2-butanone (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than---5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ( methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />