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110 2nd Avenue South,#D7,Pacheco, CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' h //www mccam bei/corn E-mail main cr mccampbell cam <br /> s <br />' Advanced GeoEnvironmental Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br />' Stockton, CA 95215 Client Contact Tun Cuellar Date Extracted 12/03-12/06/01 <br /> t Client P O Date Analyzed 12/03-12/06/01 <br /> EPA method 8260 Volatile Organics By GOMS <br />' Lab ID 84519 <br /> Client ID CPT14(93-97)/112701 <br /> Matrix W <br /> Compound * Reporting Limit Reporting Limit <br />' p Concentration W S Compound Concentration* W S <br /> Acetone Bei ND<15 50 25 trans-l,3-Dichloropropene ND 1 0 50 <br /> Benzene ND 1 0 5 0 Ethylene dibromide <br /> NO 1 0 50 <br /> Br mobenzme ND 1 0 50 Ethylbenzene NO l 0 50 <br /> Bromochlotomethane NO 10 50 Hexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 10 50 fodomethane NO 10 50 <br /> Bromoform NO 10 50 €sopmpylbenzene NO to 5 0 <br /> Bromomethane ND l 0 5 0 p-isopropyl toluene NO 1 0 ' 5 0 <br />' n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone NO 1 0 5 0 <br /> NO sec-Butyl benzene 10 5 0 Methylene Chlonde` ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone' ND 2 0 10 <br />�. Carbon Disulfide ND 1 0 5 0 Methyi isobutyl ketone NO 10 50 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlombenzene NO 1 0 50 Naphthalene NO M'I 'o <br /> 25 <br /> Chloroethane ND 1 0 5 0 n-Propyl benzene NO 5 0 <br /> 2-Chloroethyi Vinyl Ether` NO l 0 50 Styrene NO 50 <br /> Chloroform NO 1 0 5 0 1,1 1 2-TetraLhlnroethane NO 5 0 <br /> Chloromethane ND 1 0 50 1 1 2,2-Tetrachloroethane NO 5 0 <br /> 2-Chlorotoluene NO € 0 5 0 Tetiachloroethene ND 5 0 <br /> 4-ChlorotolueneND 10 5 0 Toiuene NO 1 0 5 0 <br /> DibromoLhloromethane ND 1 0 5 4 l,2,3-Tnchlorobenzene NO 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 1 20 1 10 1,2,4-Tnchlorobenzene NO 5 0 ZS <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Tnchioroethane NO l 0 50 <br /> 1,3-Dichlorobenzene NO 1 0 5 0 Tnchtoroethene ND 1 0 50 <br /> 1,4-Dichiorobenzene NO 1 0 5 0 Tnchlorofluoromethane NO 1 0 50 <br /> Dichlorodifluoromethane ND 1 6 --TO— 1,2,3-Tnchloropmpane NO 1 0 50 <br /> 1 1-Dichloroethane NO 10 50 1,2,4-Tnmethylbenzene 2 6 1 0 50 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 10 5 0 <br /> 1,1-D clilorcethene ND 1 0 50 Vinyl Acetate ° NO 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 —50 Vinyl Chloride`" ND 1 0 50 <br /> trans-l,2-Dichloroethene NO f 0 5 0 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane NO 1 0 5 0 Comments <br /> 1,3-Dichloropropane NO 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane NO 1 0 50 Dibromofluoromethane 109 <br /> 1,1-Dichloropropene ND to 50 Toiuene-l8 104 <br /> cis-l,3-Dichioropropene ND 10 50 4-Bromofluorobenzene 99 <br /> water and vapor samples arc reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> I <br /> NO means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (t) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylaeetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, {1) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> f <br />