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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAIMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> Z4 hqR//www mccampbell coni E-mail mam@mccampbell com <br /> Advanced GeoEnvironmentaI Client Project ID Three B's Date Sampled 11/26-11/27/01 <br /> 837 Shaw Road Date Received 11/30/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/03-12/06/01 <br /> I Client P O Date Analyzed 12/03-12/06/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> I Lab ID 84520 <br /> Client W CPT 14(116-119)/112701 <br /> Matrix W <br /> Reporting Limit Reporting Limit <br />' Compound Concentration" W S Compound Concentration W S <br /> Acetone{e) NDS 15 50 25 trans-1,3-Dichloropropene SID 1 0 50 <br /> Benzene ND 10 5 0 Ethylene dibromide ND 1 0 5 0 <br /> Bromobenzene ND 10 50 Ethylbenzene ND 1 0 5 0 <br /> Bromochloromethane ND 10 50 Hexachiorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND 1 0 5 0 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND l 0 50 <br /> I Bromomethane ND 1 0 5 0 p-Isopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 10 5 0 Methyl butyl ketone ND 1 0 30 <br /> sec Butyl benzene ND 10 50 Methylene Chlonde ND<2 0 1 0 50 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone 19' ND 1 0 5 0 <br /> Carbon retrachlonde ND 10 5 0 Methyl Cert-Butyl Ether(MTBE) i 1 0 50 <br /> Chlorobenzene ND 10150 <br /> Naphthalene ND 5 0 25 <br /> Chloroethane ND 1 0n-Propyl benzene ND 1 0 50 <br /> 2-Chloroethyl Vinyl Ether") ND 10Styrene' ND 1 0 50 <br /> Chloroform ND to1,1,1,2-Tetrachloroethane ND 1 0 5 0 <br /> Chloromethane ND 101,1,2 2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 10Tetrachloroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 10Toluene ND 1 0 50 <br /> Dibromochloromethane ND 101 2,3-Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibrorrio-3-chloropropane ND 2 01,2,4-Tnchlorobenzene ND 50 25 <br /> Dtbromomethane ND 101 1,I-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene Nil 10 1,1,2-Trichloroethane ND 1 0 D 0 <br /> 1,3-Dichlorobenzene ND 10Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 10Tnchlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 10 50 1 2,3-Tnehloropropane ND 10 50 <br /> 1 I-Dichloroethrme ND 10 5 0 1,2 4-Trimethylbenzene ND 1 0 50 <br /> 1,2-Dichloroethane ND 10 5 0 1 3 5-Tnmethylbenzene ND 1 0 5 0 <br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate -) ND 5 0 25 <br /> cis-1,2-Dtchloroethene ND 10 5 0 Vinyl Chlonde " ND 1 0 S 0 <br /> trans-l,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-DiLhloropropane ND 1 0 56 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 10 5 0 Dibromofluoromethane 99 <br /> 1 1-Dichloropropene ND 10 50 1 oluene-d8 105 <br /> cis-l,3-Dichloropropene ND 1 0 S Q 4-Bromotluorobenzene 98 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ugikg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> I <br /> ND means not detected above the reporting hmit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1 methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />