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110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798 1622 <br />' 4ttp!lwww mccumbell cam E mail main mccampbell corn <br /> Advanced GeoEnvironmental, Inc Client Project ID 3 B's Truck Plaza Date Sampled 06/25/03 <br />' 837 Shaw Road Date Received 06/26/03 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 06/30/03-07/02/03 <br />' Client P O Date Analyzed 06/30/03-07102/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0306567 <br />' Lab ID 0306567-OOIB 0306567-002B ' 0306567-003B 0306567-004B <br /> Client ID DW-1 MW1 MW2 MW3 Reporting Limit for <br /> Matrix W W I W W DF=1 <br /> DF I 33 40 100 S W <br />' Compound Concentration ug/kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND<17 ND<20 ND<50 NA 05 <br />' Benzene ND 970 1400 2800 NA 05 <br /> t-Butyl alcohol(TBA) ND ND<170 ND<200 ND<500 NA 50 <br />' 1,2-Dibromoethane(EDB) ND ND<17 ND<20 77 NA 05 <br /> 1,2-Dichlorocthane(1,2-DCA) ND ND<17 ND<20 ND<50 NA 05 <br />' . Dusopropyl ether(DIPE) ND ND<17 ND<20 ND<50 NA 05 <br /> Ethylbenzene ND 52 130 460 NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND ND<17 ND<20 ND<50 NA 05 <br /> IMethyl-t-butyl ether(MTBE) ND ND<17 23 ND<50 NA 05 <br /> Toluene ND 38 78 470 NA 0 5 <br />' Xylenes ND l30 180 1400 NA 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI 102 105 120 101 <br /> %SS2 95 6 960 969 97 2 <br /> %SS3 108 101 899 961 <br />' Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in pg/kg, wipe samples inµglwlpe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> 4 surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,l)sample diluted due to high <br /> ,organic content <br /> DHS Certification No 1644 Angela Rydelms,Lab Manager <br /> I <br />