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110 2nd Avenue South,#D7,Pacheco CA 94553 5560 <br /> McCampbell Analytical Inc I Telephone 925-798-1620 Fax 925-798-1622 <br />' 24 http l/www niccampbeIl com E-mail rnaT@rnccarnpbcIl corn <br /> Advanced GeoEnvlronmental,Inc Client Project ID Three B's Date Sampled 06/25/03-06126/03 <br />' 837 Shaw Road Date Received 06/27/03 <br /> Stockton,CA 95215 Client Contact Turn Cuellar Date Extracted 07/02103-07103/03 <br />' rChent P O Date Analyzed 07/02/03-07/03103 <br /> Oxygenates and BTEX by GC/MS* <br /> Extractum Method SW503013 Analytical Method SW0260B Work Order 0306602 <br />' Lab ID 0306602-OOIB 0306602-002B 0306602-003B 0306602-004B <br /> € E <br /> Client 1D MW4 MW5 MWl le <br /> MW l if Reporting Limit for <br />' Matrix W W W W DF=1 <br /> DF 25 i 1 - 1 j WLLT S W <br />' Compound Concentration u <br /> Fes$ pP�L <br /> Cert-Amyl methyl ether(TAME) ND<l 2 I ND ND ANDNA <br /> 05 <br />' Benzene ND<l 2 57 ND 05 <br /> t-Butyl alcohol(TBA) ND<12 48 ND 50 <br /> I1,2-Dibromoethane(EDB) ND<l 2 ND ND 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND<l 2 ND ND 05 <br />'. Dusopropyl ether(DIPE) ND<I 2 ND ND —ND NA 05 <br /> Ethylbenzene ND<I 2 ND ND ND NA 05 <br /> Ethyl tert-butyl other{ETRE) ND<1 2 ND ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) 70 ND ND ND NA 05 <br /> Toluene ND<1 2 ND ND ND NA 05 <br /> Xylenes ND<l 2 ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SSI 106 106 107 109 <br /> %SS2 985 972 985 98 1 <br /> %SS3 104 106 106 106 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soillsludgelsohd samples in pglkg, wipe samples in gg/wipe, <br /> productloil/non-aqueous liquid samples in mg/L. <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than–2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> IDHS Certification No 1644 /� _ Angela Rydehus,Lab Manager <br />