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1 <br /> 110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925 798-1622 <br />' A# ht(pJ/www rmcarripbell com E mail morn ca bell corn <br /> Advanced GeoEnviromnental,Inc Client Project ID Three B's Date Sampled 06125/03-06/26/03 <br />' 837 Shaw Road Date Received 06/27/03 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 07/02/03.07/03/03 <br />' Client P O Date Analyzed 07/02/03-07/03/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW503m Analytical Method SW8260B Work Order 0306602 <br />' Lab ID 0306602-005B i 0306602-006B 0306602-007B 0306602-008B <br /> Client ID MW10f MWI0C MW10d MW10c <br /> Reporting Limit for <br /> Matrix W € W W W DF=1 <br /> DF S W <br />' Compound Concentration ug/kg ug/L <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> Benzene 099 0 70 0 58 6 3 NA 0 5 <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 5 0 <br /> 1,2-Dtbromoethane(EDB) ND ND ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND NA 05 <br /> Dilsopropyl ether(RIPE) ND ND ND ND NA 0 5 <br /> Ethylbenzene ND ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) ND ND ND I I NA 0 5 <br /> Toluene ND ND ND ND NA 0 5 <br /> Xylenes ND ND ND ND NA 0 5 <br /> Surrogate Recovenes(%) <br /> %SSI 109 108 107 109 <br /> %SS2 98 7 100 100 979 <br /> %SS3 105 104 105 113 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/salid samples to Vg/kg, wipe samples to jig/wipe, <br /> product/oil/nan-aqueous liquid samples in mg/1— <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,3)sample diluted due to high <br /> organic content <br /> 1 <br /> DHS Certification No 1644 _ Angela Rydehus, Lab Manager <br />