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1 <br /> 110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> MCCampbell Analytical IncTelephone 925-798-1620 Fax 925 798 1622 <br />' h llwww mcc bell com E mail num@rmcanipbell cam <br /> Advanced GeoEnvironmental, Inc Client Project ID Three B's Date Sampled 06/27/03 <br />' 837 Shaw Road Date Received 07/01/03 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 07/07/03 <br /> Client P O Date Analyzed 07/07/03 <br /> Oxygenated Volatile Organics+EDS and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0307006 <br /> Lab ID 0307006-OOIC 0307006-002C 0307006-003C 0307006-004C <br /> Client ID MW11A MW11B MW12A MW12B <br /> Reporting Limit for <br />' <br /> Matrix W W W W DF=I <br /> DF 1 ] 1 - —_i--- S w <br />' Compound Concentration ug/kg gg/L <br /> Diisopropyl ether(DIPE) ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETRE) ND ND ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) 25 074 ND 051 NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br />'• t-Butyl alcohol(TBA) 66 ND ND ND NA 50 <br />' 12-Dibromoethane(EDB) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) 36 ND ND ND NA 05 <br />' Surrogate Recoveries(%) <br /> %SS 109 111 110 110 <br />' Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soiVsludge/solid samples inµg/kg, wipe samples in pg/wipe, <br /> product/oil/non-aqueous liquid samples m mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> I <br /> • <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />