I
<br /> Jan C9 2004 12: 13PM Mc` gl*IPBELL - ANALYTICAL 'INC 325'7q.84612 p.7
<br /> 110 tad Avenue Sovrh,#07,Pacheco,CA 94553-SS60
<br /> McCwnpbell Analytical Inc. Telephone x;925-798-[620 Fax:925-718-1622-'
<br /> ��" h Jlwww.mcc il.conr �urarT:main c Il.com
<br /> Ceres Associates Client Project ID: #CAL156-2 Date Sampled: 01/07/04
<br /> 555 First Street,Ste.303 Date Received: .01/07/04
<br /> Client Contact: Ryan Meyer Date Extracted: 01/07/04
<br /> Benicia,CA 94510
<br /> Clierrt P.O.: Date Analyzed: 01/07/04
<br /> Volatiles Organics by P&T and GC/MS(Basic Target hist)*
<br /> ExnetboMetbod: SW503CE Analytical Method: SW82609 - Work Order:0401042
<br /> Lab ID 0401042-006A _
<br /> Client ID SB2-5 l
<br /> Matrix Soil
<br /> Compound Concentration* DF Compound 'i Concentration* s DF
<br /> Acetone ND t.0 50 Benzene NO 1.0 5.0
<br /> Bromobenzene ND 1.0 5.0 Bromochlaromethane ltiD 1.0 5.0
<br /> Bromodichloromethane ND, 1.0 5.0 1 Bromofotm \U 1.0 5.0
<br /> 2-Butanane(MM ND 1.0 10 Bromomcthane ND' 1.0 5.0
<br /> -n-Butyl benzene: ND 1.0 5.0 sec-$u l benzene ND 1.0 5.0
<br /> tert-Butyl benzene ND 1_0 5.0 Carbon Disulfide ND 1.0 5.0
<br /> Carbon Tetrachloride ND 1.0 5.0 Chlorobenzene ND 1.0 5.0
<br /> Chlmoethanc ND 1 1.0 5.0 2-Chloroeth'I Vinyl Ether ND 1.0' 10
<br /> Chloroform ND L.0 5.0 Chioromethanc ND 1.0 5.0
<br /> ' 2-Chlorotoluene ND 1.0 5.0 4-Chlorotoluene ND 1.0 5.0
<br /> Dibromochlorvtnethane ND - 1.0 5.0 1,2-Dibromo-3-chloro m'ana ND 1.0 5.0
<br /> 1,2-Dibromoethane D13ND L.0 5.0 Dibromomdhane ND I.0 i '5.0
<br /> 1,2-Dichlorobenzene ND 1.0 5.0 1 1,3-Dichlorobenzene ND 1.0 : 5.0
<br /> L 1,4-Dichloruba=ne ND 1.0 5.0 Dichloroditluaromethane r ND 1.0 5.0
<br /> -1,1-Dichloroathama ND 1.0 5.0 1,2-Dicb1oroetlu=(1,2-DCA) NO 1.0 5.0
<br /> 1,1 Dichloroetheue ND 1.0 5.0 cis-1 2-DiAloroethene ND Lot 5.0
<br /> trairts-l,2-Dichlosoothenc ND l.0 5.0 1,2-13ichioro a ane ND 1.0 5.0
<br /> 1,3-Dicb1oroprargafte ND 1.0 5.0 2,2-Dichloro ro ane ND 1.0 5.0
<br /> 1,1-Dichloroene ND 1.0 5.0 cis-1,3-Dichloroene ND 1.0 5.0
<br /> trans-1,3-11chloro ne ND 1.0 5.0 1 Eth ]benzene AID 1.0 5.0
<br /> Hexachlurobutadiene AID 1.0 5.0 2-Hcxanone ND 1.0 5.0
<br /> Iadomethane(Methyl iodide AID 1.0 SO Isoworrylbenzene ND 110 15.0
<br /> 4-tsa 1 toluene ND 1.0 5.0 Methyl-t-but I ether TBE NO 1.0 5.0
<br /> Meth lenechloride ND 1.0 5.0 4-Math I-2- entanone(MIBK) ND 1.0 5.0
<br /> Na hth.Ocne ND 1.0 5.0 n-Prov 1benzene ND 1.0 5.0
<br /> Styrene ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0
<br /> 1,1,2 2-Tetrachloroethane ND 1.0 5.0 Te rachlomethene ND 1.0 5.0
<br /> Toluene ND 1.0 5.0 1,2,3-Trichlarobenzenc ND 1.0 5.0
<br /> 1,2,4-Trichlarubenzene ND 1.0 5,0 1,1,]Trichloroethane ND 1.0 5.0
<br /> 1,1,2-Trichloroethane ND 1.0 5.0 Trichloroethene ND 1,0 5.0
<br /> Trichlorofluoromethane ND 1.0 5.0 1,2,3-Trichlaro a ane ND 1,4 5.0
<br /> L,2,4-Trimclts ]benzene ND lA 5.0 1,3,5-Trimeth (benzene ND. 1.0 5.0
<br /> Yin i Acetate ND - 1.0 ! 50 Vin 1 Chtoride ND l A 5.0
<br /> Xylenes ND 1.0 5.0
<br /> 5urrogste,Recoveries(%),
<br /> °hSS1: 93.3 %SS2; 96.8
<br /> /DSS3: 104
<br /> Comments:
<br /> •water and vapor samples and all TCLP&SPLP extracts are reported inµglL,soil/sludgelsolid samples'inµg/kg, wipe samples inµglwipe,
<br /> praduct/oWrion-aqueous liquid samples in mg/L.
<br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis.
<br /> �j 1F surrogate diluted out of range or surrogate coetutes with another peak.
<br /> h)lighter than water immiscible sheenlproducl is presort;i)liquid sample that contains greater than-2 vol.%sediment;j}sample diluted due to high
<br /> organic content.
<br /> DHS Cerlificatian No. 1644 ela Rydelius,Lab Manager
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