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Jan 09 2004 12: 14PM Me 'IMPBELL 19NALYTICFIL INC 925T 4612 P- El <br /> 1102nd Averwe Suath,#07,Pac"hem,CA 94553-55 60 <br /> a McCampbell Analytical Inc. Telephone:925-79s-162a Fan:925.798-1622 <br /> ,�"7� h rllwww.rrue ell.com B•meil:m►ima c ll.eom <br /> Ceres Associates Client Project ID: #CA1156-2 Date Sampled; 01/07/04 <br /> 555 First Street,Ste.303 Date Received: 01107f04 <br /> Client Contact: Ryan Meyer Date Extracted: 01/07/04 <br /> Benicia,CA 94510 <br /> Client P.O.: Date Analyzed: 01/07/04 <br /> F <br /> Volatiles Organics by P&T and GCIMS(Basic Target List)* <br /> Exwacdon Mc1hod: SW5030B Analytical Method: SW8260B Werk Order.D401042 <br /> Lab ID 0401042-008A <br /> Client ID I SB3-5 <br /> Matrix Soil <br /> Compound Concentration' DF ' t kati s Conwoun Concentration#1:S DP '�P=nit s <br /> ' Aeetnne ND 1.0 50. Benzene ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Bromoc-MOrornethane ND 1.0 5.0 <br /> Bromodichloromethane ND 1.0 5.0 Broroofomi ND 1.0 5.0 <br /> 2-Butuwne MIEK ND - 1.0 t0. Bromorrethane ND 1.0 5.0 <br /> n B 1benzene ND 1.0 5.0 sec-But banienc ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Carbon Disulfide NO 1.0 5.0 <br /> Carboa Tetrachloride ND 1.0 5.0 Chloroben-mne ND 1.0 5-0 <br /> Chloroetbane ND 1.0 5.0 2-Chloroeth 1 Vin l Ether ND 1.0 10 <br /> Chloroform ND 1.0 5.0 Chloromethane ND 1.0 S.0 <br /> 2-Chlorotoluerte ND 1.0 5.0 4-Chlorotoluene ND 1.0 5.0 <br /> Dibrornnhloromethane ND 1.0 5.0 1,2-Dihmmo-3-chloro ro` t ND 1.0 5.0 <br /> 12-1]ibromoothanc EDS ND 1.0 5.0 Dibramomrthane ND 1.0 5.0 <br /> 1,2-Diohloroberizam ND 1.0 "5.0 1,3-Dichlorobenzene ND 1.0 5.0 <br /> 1,4-Diehlorobertzerm ND 1.0 5.0 Dichlorodifluoromethane ND 1.0 5.0 <br /> 1 1 Dichlorocthane ND 1 1.0 _ 1 5.0 1,2 Dichlomethane 1 -DCA) ND 1.0 5.0 <br /> 1,1Diehloroethene, ND 1.0. 5.0 cis-1,2-Dichloroethen6 ND -1.0 S.0 <br /> trans-1,2-Dichlorocthene ND 1.0 5.0 l,2-Dichloroane ND 1.0 5.0 <br /> L 3-Dichloro ro ane ND 1.0 5.0 2,2-Dicblom o ane ND 1.0 5.0 <br /> -l.l-Dicb1()TolM9pcnc ND 1.0 5.4 cis-t,3-Dichlona o ene ND 110 5.0 <br /> trans-1,3-Dichloro ene ND 1.0 5.0. Eth lbenzene ND 1.0 5.0 <br /> Hexachlorobutadiene ND I.0 5.9 2-flexanone ND 1A ..5.0 <br /> LIodomethane Meth'I iodide ND 1.0 50 1 Iso ry ylber=ne ND I'D 5.0 <br /> 4-Iso i toluene ND 1.0 5.0 Meth 1-t-but ether MTBLe ND 1.0 5.0 <br /> Methylene chloride ND 1.0 5.0 4-Meth l-2 ntanone K ND i.0 5.0 <br /> Na hthalme ND _1.0 5.0 n-Pyopyl benzene ND 1.0 5,0 <br /> Styrene 1,1,1,2-Tetrachloroethane ND 1,0 5.0 <br /> 1,1 2-Tetrachloroethane ND 1.0 5.0 Tettachloroethena ND 110 5-0- <br /> Toluene <br /> '.0Toluene ND 1.0 i3O 1,2,3-Trichlorobmzene ND 1.0 5.0 <br /> 1,2,4-Triclalorobenzene ND l.0 5.0 1.1.1-Trichloruethane ND 1.0 5.0 <br /> 1,1,2=Triah1oroethww ND 1.0 5.0 Trichloroethene ND l.o ,5.1D <br /> Trichlorofluoromethane ND 1.0 5,0 1,2,3 Trichlam ra ane ND 1 1.0 8.0 <br /> 12,4-Trimelh ibenzene ND 1.0 5.0 1,3,5-Trimeth lbenzene ND 1.0 5.0 <br /> Vinyl Acetate ND 1.0 50 Vinyl Chloride ND 1.0 5.0 <br /> Xylenes NO 1.0 5.0 <br /> Surrogate Recoverles(°Jo) <br /> %SSl: 92.6 °Jo552: 96.6 <br />'4 %S53: 103. <br /> L Comments: ' <br /> *water and vapor samples and all TCLP&5PLP extracts are reported inµglL,soil/sludge)solid samples in 4Wkg, wipe samples inµg/wipe, <br /> product/pi/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis, <br /> #surrogate diluted out of range or surra ate s <br /> cuelutewith another peak. <br /> g 8 8 <br /> h)lighter than water immiscible sheenlproduct is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br />. or is content. <br /> DHS Certification No. 1644 eia Rydelius,Lab Manager <br />