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110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> Inc.McCampbell Analytical, Telephone 925 798 1620 Fax 925 798 1622 <br /> Website www mccampbell corn E-mail mam@mecampbell com . <br /> Port of Stockton Client Project ID Port of Stockton UST Date Sampled 06/01/05 , <br /> Site No 3 <br /> P O Box 2089 Date Received 06/03/05 <br /> Client Contact Rita Koehnen Date Extracted 06/04/05 <br /> Stockton,CA 95201-2089 <br /> Client P70 Date Analyzed 06/04/05 <br /> MTBE and BTEX by GC/MS* , <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0506068 <br /> Lab ID 0506068-OOIB 0506068-002B 0506068-003B 0506068-004B <br /> Client ID MW 3-1 MW 3-2 MW 3-3 MW 3-4 ' <br /> Reporting Limit for <br /> Matrix - - -W -W --W- - DF=1 <br /> DF 1 10 10 1 S w , <br /> Compound Concentration ug/kg µg/L <br /> Benzene ND 55 ND<5 0 ND NA 0 5 , <br /> Ethylbenzene 79 41 45 ND NA 05 <br /> Toluene 13 150 150 ND NA 0 5 ' <br /> Xylenes 40 290 260 ND NA 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI 98 95 93 93 ' <br /> -%SS2�- _ ---95 --96 = 94— ==95- <br /> %SS3 - —_-� _F -- 94 � 96 95 96 <br /> Comrinettts - T <br /> •water and vapor samples are reported inµg/L,soil/sludge/solid samples in mg/kg,product/oiUnon-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in 4wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or coelutes with another peak,&)low surrogate due to matrix interference ' <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-1 vol O/a sediment,,])sample diluted due to high <br /> organic eontent/matnx interference k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) , <br /> peporting limit raised due to insufficient sample amount,n results are reported on a dry weight basis, see attached narrative <br /> i <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br />