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110 2nd Avenue South 4D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798 1620 Fax 925 798 1622 <br /> 4. Website www mccampbell com E[nail mam mccampbetl cam <br /> Port of Stockton Client Project ID Port of Stockton UST Date Sampled 06/01/05 <br /> Site No 3 <br /> P O Box 2089 Date Received 06/03/05 <br /> Stockton,CA 95201-2084 Client Contact Rita Koehnen Date Extracted 06/04/05 <br /> Client P O Date Analyzed 06/04/05 <br />' MTBE and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW9260B Work Order 0506068 <br /> Lab ID 0506068-005B 0506068-006B 0506068-0078 <br />' Client ID MW 3-5 MW 3-6 Trip Blank Reporting Limit for <br /> Matrix W W W DF=1 <br /> DF 1 100 1 S W <br /> Compound Concentration ug/kg µg/L <br />' Benzene ND 1000 ND NA 0 5 <br /> Ethylbenzene ND ND<50 ND NA 0 5 <br /> Toluene ND ND<50 ND NA 0 5 <br /> Xylenes ND ND<50 ND NA 05 <br /> Surrogate Recoveries(%} <br /> %SSI 90 93 92 <br /> %SS2 94 95 116 <br />' %SS3 99 99 101 <br /> Comments <br /> *water and vapor samples are reported inµglL soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported to mg/1,,wipe samples in yg/wipe <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or coelutes with another peak &)low surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,1)liquid sample that contains greater than—1 vol %sediment,j)sample diluted due to high <br /> organic content/matrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight,m) <br /> reporting lim it raised due to insufficient sample amount n results are reported on a dry weight basis see attached narrative <br /> 1 <br /> • <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />