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a., <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell AInc.4 nalytical, Telephone:925-799-1620 Pax:925-798-1622 <br /> Website:www.mccanrpbel4.com E-mail:rrain�]amccwMbell.00m <br /> WGR Southwest,Inc. Client Project TD: Port of Stockton UST Date Sampled: 09/23/04 <br /> Site No.3 <br /> Le <br /> 315 W.Pine Street, Suite 1A Date Received: 09/24/04 <br /> Client Contact: Jim Neal Date Extracted: 09/25/04-09/28104 <br /> Lodi,CA 95240 <br /> Client P.O.: Date Analyzed: 09/25/04-09128104 <br /> MTBE and BTEX by GC/MS* <br /> Exmcdon Method:SW5030B Analytical Melhod:SW8260B Work Order:0409382 <br /> i, Lab ID 0409382-OOID 0409382-002B 0409382-00313 0409382-004B <br /> _...__..._...._..._...._._._..-----..---_-----_... <br /> ---.--.------............ ----- <br /> Client 1D MW 3-1 MW 3-2 MW 3-4 MW 3 5 Reporting Limit for <br /> Matrix W W W W DF=1 <br /> I <br /> DF 1 33 1 I 1 S w <br /> I <br /> Compound Concentration ug/kg µg/L <br /> Benzene 1.0 300 ND ND NA 0.5 <br /> V Ethylbenzene 27 330 ND ND NA 0.5 <br /> Methyl-t-butyl ether(MTBE) ND ND<17 ND ND NA 05 <br /> i.+ <br /> i <br /> Toluene 27 1300 ND ND NA 0.5 <br /> I . <br /> Lr Xylenes 50 1500 I ND ND NA 0.5 <br /> I <br /> Surrogate Recoveries(%) <br /> j.. %531: 109 I 108 11.0 108 <br /> %SS2: 103 105 102 103 <br /> LO <br /> %SS3: 114 114 117 I 117 <br /> � 1 <br /> Comments -- <br /> La <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soillstudgelsolid samples in pg/kg, wipe samples inµg/wipe, <br /> prod uct/oillnon-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> 16a <br /> #surrogate diluted out o€range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than—1 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> LO <br /> I.r <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />