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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone;925-798-1620 Fax:925-798-1622 + <br /> Website:www.mecampbell,com E-mail:main@3ttecanrpbel1rom <br /> W GR Southwest,Inc. Client Project ID: Port of Stockton UST Date Sampled: 09/23/04 <br /> Site No.3 <br /> 315 W.Pine Street, Suite 1A Date Received: 09/24/04 <br /> CIient Contact: Jim Neal Date Extracted: 09125/04-09/28/04 <br /> Lodi, CA 95240 <br /> Client P.O.: Date Analyzed: 09/25/04-09128104 <br /> MTBE and BTEX by GC/MS* <br /> Extraction Method:SW5030B Analytical Method!SW8260B Work Order:0409382 <br /> Lab 1D 0409382-005B <br /> I <br /> ------------- <br /> Client ID MW 3-6 <br /> Reporting Limit for <br /> MatrixW D1:41 <br /> DF 50 S W <br /> t <br /> Compound Concentration ug/kg ltg/L <br /> Benzene 1800 NA 0.5 i <br /> I <br /> Ethylbenzene 33 I NA 0.5 <br /> I <br /> Methyl-t-butyl ether(MTBE) Np[25 NA 0.5 <br /> I <br /> Toluene 43 NA 0.5 <br /> Xylenes 160 i NA 0.5 <br /> Surrogate Recoveries(%} <br /> %551' 106 <br /> i <br /> %SS2: 105 <br /> %SS3: 119 <br /> Comments f i <br /> i <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soillsludge/solid samples inµg/kg, wipe samples in pg/wipe, w <br /> product/oillnon-aqueous liquid samples in mg/L. <br /> I�ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> #surrogate diLted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than—1 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />