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IN ACCpR0 <br /> stone 4p� q'y�F MEMBER <br />� LfeyU <br /> . LABORATORIES, INC <br /> GeoSyntec-Oakland Project Western Farm Service-Vernalis <br /> 475 14th Street,Suite 450 Project Number [none] Reported <br />' Oakland CA,94612 Project Manager Susan Skoe 12/10/04 08 59 <br /> Determination of Permanent Gases-Quality Control <br /> jKeystone Laboratories, )Inc. -Newton <br /> Repotting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 1L40137-Perm Gases <br /> Calibration Check(IL40137-CCV2) Prepared&Analyzed 12/01/04 <br /> Ethylene 2583 m9/1 2170 119 70-130 <br /> Ethane 2852 2330 122 70-130 <br /> Methane 1551 12,30 126 70-130 <br /> Duplicate(I1A0137-DUP1) Source 14KI171-01 Prepared&Analyzed 12/01/04 <br /> Ethylene ND 0 008 mg/1 ND 30 <br /> Ethane ND 0 008 ND 30 <br /> Methane 00762 0 005 0 077 104 19 <br /> Batch 1L40138-Perm Gases <br /> Blank(1L40138-BLKI) Prepared&Analyzed 12/01/04 <br /> Fn Dioxide ND 0 020 mg/l <br /> LIPS(1L40138-BSI) Prepared&Analyzed 12/01/04 <br /> Carbon Dioxide 3020 mg/l 3410 886 62-131 <br /> Calibration Check(IL40138-CCV1) Prepared&Analyzed 12/01/04 <br /> Carbon Dioxide 2690 mg/l 3410 789 70-130 <br /> lCalibration Check(1L40138-CCV2) Prepared&Analyzed 12/01/04 <br /> Carbon Dioxide 2990 mg/l 341 0 877 70-130 <br /> Duplicate(IL40138-DUPI) Source 14KI101-01 Prepared&Analyzed 12/01/04 <br /> Carbon Dioxide 1926 0 020 mg/l 203 526 18 <br /> 1 stone Laboratories, Inc -Newton The results in this report apply to the samples analyzed in accordance with the chain of <br /> it custody document Thu analytical report must be reproduced in its entirety <br /> Jeffrey Kung,Ph D,Laboratory Director page 10 of 23 <br /> Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 <br /> Newton, IA 50208 <br />