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1 <br /> �o`��Q �N A C C p�09ycE <br /> stoneCi MEMBER <br /> I* LABORATORIES, INC a <br />' GeoSyntec-Oakland Project Western Farm Service-Vernalis <br /> 475 14th Street,Suite 450 Project Number [none] Reported <br />' Oakland CA,94612 Project Manager Susan Skoe 12/10/04 08 59 <br /> Determination of Metabolic Acids- Quality Control <br /> Keystone Laboratories, Inc. - Newton <br /> Reporting Spice Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />'Batch 1L40920-General Prep HPLCAC <br /> Blank(1L40920-BLKI) Prepared&Analyzed 12/08/04 <br />'Pyruvic Acid(0) ND 0 t mg(l <br /> Lactic Acid(C3) ND 10 " <br /> Acetic Acid(C2) ND 10 <br /> Propionic Acid(0) ND 10 " <br />'Butyric Acid(C4) ND to " <br /> LCS(IL40920-BSI) Prepared&Analyzed 12/08/04 <br /> Pyruvic Acid(C3) 1955 0 t mg/l 2030 963 72-137 <br /> Lactic Acrd(C3) 8l 50 l 0 9308 876 72-122 <br /> Acetic Acid(C2) 1018 1 0 1062 959 88-126 <br /> Propionic Acid(0) 9888 to " 1005 984 90-117 <br /> nc Acid(C4) 1009 10 1020 989 86420 <br /> Dup(1L40920-BSD1) Prepared 12/08/04 Analyzed 12/09/04 <br /> Pyruvic Acrd(C3) l9 84 01 mgA 2030 97 7 72-137 147 18 <br /> Lactic Acid(C3) 83 61 l 0 9308 898 72-122 256 10 <br />(Acetic Acid(C2) 1034 10 1062 974 88-126 156 I5 <br /> Propionic Acid(0) 1024 t 0 1005 102 90-117 3 50 12 <br /> Butyric Acid(C4) 1023 10 1020 100 86-120 138 13 <br />'Calibration Check(1L40920-CCV1) Prepared&Analyzed 12/08/04 <br /> Pyruvic Acrd(0) 1679 01 mgA 1500 112 80-120 <br /> Lactic Acid(0) 8005 10 9469 845 80-120 <br />'Acetic Acrd(C2) 1097 to 1030 107 80-120 <br /> Propionic Acid(C3) 1045 10 1005 104 80-120 <br /> Butyric Acid(C4) t 12 5 to " 1103 102 80-120 <br />'Calibration Check(IL40920-CCV2) Prepared 12/08/04 Analyzed 12/09/04 <br /> Pyruvic Acid(0) t7 26 01 mgA 1500 115 80-120 <br /> Lactic Acid(C3) 8141 1 0 9469 860 80-120 <br /> Acetic Acid(C2) t 10 6 to 103 0 107 80-120 <br />'Propionic Acrd(0) 1073 to " 100 5 107 80-120 <br /> Butyric Acid(C4) t 17 3 to 1103 106 80-120 <br /> 1 <br /> 1 Keystone Laboratories, Inc -Newton The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br /> 1 � <br /> Jeffrey King,Ph D,Laboratory Director Page I 1 of 23 <br /> 1 Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 <br /> Newton, IA 50208 <br />