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Laboratories Inc. _ <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/28/2016 17:22 <br /> 3590 Iron Court Project: Diamond Pet Foods-COELT <br /> Shasta Lake City,CA 96019 Project Number: 010107.08 Task 4 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> Quality Control Report - Precision & Accuracy <br /> Control Limits <br /> Source Source Spike Percent Percent Lab <br /> Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Quals <br /> QC Batch ID: BZJ1056 Used client sample: Y-Description: 013-1, 10/11/2016 09:50 <br /> Chloride DUP 1628545-01 12.447 12.414 mg/L 0.3 10 <br /> MS 1628545-01 12.447 64.677 50.505 mg/L 103 80-120 <br /> MSD 1628545-01 12.447 65.229 50.505 mg/L 0.9 105 10 80-120 <br /> Nitrate as N DUP 1628545-01 7.4070 7.2550 mg/L 2.1 10 <br /> MS 1628545-01 7.4070 12.246 5.0505 mg/L 95.8 80-120 <br /> MSD 1628545-01 7.4070 12.445 5.0505 mg/L 1.6 99.8 10 80-120 <br /> Sulfate DUP 1628545-01 58.909 58.332 mg/L 1.0 10 <br /> MS 1628545-01 58.909 165.58 101.01 mg/L 106 80-120 <br /> MSD 1628545-01 58.909 166.56 101.01 mg/L 0.6 107 10 80-120 <br /> QC Batch ID: BZJ1057 Used client sample: Y-Description: 013-22, 10/11/2016 14:14 <br /> Chloride DUP 1628545-11 2.8440 2.7060 mg/L 5.0 10 <br /> MS 1628545-11 2.8440 54.421 50.505 mg/L 102 80-120 <br /> MSD 1628545-11 2.8440 54.569 50.505 mg/L 0.3 102 10 80-120 <br /> Nitrate as N DUP 1628545-11 ND ND mg/L 10 <br /> MS 1628545-11 ND 5.1535 5.0505 mg/L 102 80-120 <br /> MSD 1628545-11 ND 5.1747 5.0505 mg/L 0.4 102 10 80-120 <br /> Sulfate DUP 1628545-11 3.9970 3.8170 mg/L 4.6 10 <br /> MS 1628545-11 3.9970 107.04 101.01 mg/L 102 80-120 <br /> MSD 1628545-11 3.9970 107.38 101.01 mg/L 0.3 102 10 80-120 <br /> QC Batch ID: BZJ1198 Used client sample: N <br /> Bicarbonate DUP 1628533-01 76.424 76.424 mg/L 0 10 <br /> Carbonate DUP 1628533-01 ND ND mg/L 10 <br /> pH DUP 1628533-01 8.1100 8.1200 pH Units 0.1 20 <br /> Electrical Conductivity @ 25 C DUP 1628533-01 314.00 314.90 umhos/cm 0.3 10 <br /> QC Batch ID: BZJ1199 Used client sample: Y-Description: OB-4, 10/11/2016 12:58 <br /> Bicarbonate DUP 1628545-03 828.04 835.08 mg/L 0.8 10 <br /> Carbonate DUP 1628545-03 ND ND mg/L 10 <br /> pH DUP 1628545-03 7.8400 8.0000 pH Units 2.0 20 <br /> Electrical Conductivity @ 25 C DUP 1628545-03 2512.0 2523.3 umhos/cm 0.4 10 <br /> QC Batch ID: BZJ1200 Used client sample: Y-Description: 013-25, 10/11/2016 10:00 <br /> Bicarbonate DUP 1628545-13 380.26 382.49 mg/L 0.6 10 <br /> Carbonate DUP 1628545-13 ND ND mg/L 10 <br /> pH DUP 1628545-13 7.6100 7.6500 pH Units 0.5 20 <br /> Electrical Conductivity @ 25 C DUP 1628545-13 1774.7 1773.0 umhos/cm 0.1 10 <br /> QC Batch ID: BZJ1427 Used client sample: Y-Description: 013-4, 10/11/2016 12:58 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party. BC Laboratories,Inc.assumes no responsibility for report alteration,separation,detachment or third party interpretation. <br /> Report ID: 1000538621 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 54 of 59 <br />