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Laboratories Inc. _ <br /> Environmental Testing Laboratory Since 1949 <br /> Lawrence&Associates Reported: 10/28/2016 17:22 <br /> 3590 Iron Court Project: Diamond Pet Foods-COELT <br /> Shasta Lake City,CA 96019 Project Number: 010107.08 Task 4 <br /> Project Manager: David Kirk <br /> Water Analysis (General Chemistry) <br /> Quality Control Report - Precision & Accuracy <br /> Control Limits <br /> Source Source Spike Percent Percent Lab <br /> Constituent Type Sample ID Result Result Added Units RPD Recovery RPD Recovery Quals <br /> QC Batch ID: BZJ1427 Used client sample: Y-Description: OB-4, 10/11/2016 12:58 <br /> Total Dissolved Solids @ 180 C DUP 1628545-03 1410.0 1410.0 mg/L 0 10 <br /> QC Batch ID: BZJ1428 Used client sample: Y-Description: OB-24, 10/11/2016 09:40 <br /> Total Dissolved Solids @ 180 C DUP 1628545-12 785.00 800.00 mg/L 1.9 10 <br /> QC Batch ID: BZJ1517 Used client sample: Y-Description: 013-1, 10/11/2016 09:50 <br /> Total Kjeldahl Nitrogen DUP 1628545-01 0.21220 0.11920 mg/L 56.1 20 J,A02 <br /> MS 1628545-01 0.21220 2.1761 2.0000 mg/L 98.2 90-110 <br /> MSD 1628545-01 0.21220 2.2640 2.0000 mg/L 4.0 103 20 90-110 <br /> QC Batch ID: BZJ1605 Used client sample: Y-Description: OB-1, 10/11/2016 09:50 <br /> Dissolved Calcium DUP 1628545-01 69.425 68.860 mg/L 0.8 20 <br /> MS 1628545-01 69.425 75.812 10.204 mg/L 62.6 85-115 A03 <br /> MSD 1628545-01 69.425 77.305 10.204 mg/L 2.0 77.2 20 85-115 A03 <br /> Dissolved Magnesium DUP 1628545-01 25.473 24.900 mg/L 2.3 20 <br /> MS 1628545-01 25.473 34.620 10.204 mg/L 89.6 85-115 <br /> MSD 1628545-01 25.473 34.413 10.204 mg/L 0.6 87.6 20 85-115 <br /> Dissolved Sodium DUP 1628545-01 175.46 172.65 mg/L 1.6 20 <br /> MS 1628545-01 175.46 176.58 10.204 mg/L 11.0 85-115 A03 <br /> MSD 1628545-01 175.46 176.59 10.204 mg/L 0.0 11.1 20 85-115 A03 <br /> Dissolved Potassium DUP 1628545-01 6.2203 6.0936 mg/L 2.1 20 <br /> MS 1628545-01 6.2203 16.423 10.204 mg/L 100 85-115 <br /> MSD 1628545-01 6.2203 16.666 10.204 mg/L 1.5 102 20 85-115 <br /> QC Batch ID: BZJ1606 Used client sample: Y-Description: OB-22, 10/11/2016 14:14 <br /> Dissolved Calcium DUP 1628545-11 2.6625 2.6704 mg/L 0.3 20 <br /> MS 1628545-11 2.6625 14.046 10.204 mg/L 112 85-115 <br /> MSD 1628545-11 2.6625 14.126 10.204 mg/L 0.6 112 20 85-115 <br /> Dissolved Magnesium DUP 1628545-11 0.92899 0.95973 mg/L 3.3 20 <br /> MS 1628545-11 0.92899 12.333 10.204 mg/L 112 85-115 <br /> MSD 1628545-11 0.92899 12.052 10.204 mg/L 2.3 109 20 85-115 <br /> Dissolved Sodium DUP 1628545-11 32.792 33.534 mg/L 2.2 20 <br /> MS 1628545-11 32.792 42.647 10.204 mg/L 96.6 85-115 <br /> MSD 1628545-11 32.792 42.425 10.204 mg/L 0.5 94.4 20 85-115 <br /> Dissolved Potassium DUP 1628545-11 0.58289 0.63491 mg/L 8.5 20 J <br /> MS 1628545-11 0.58289 11.262 10.204 mg/L 105 85-115 <br /> MSD 1628545-11 0.58289 11.229 10.204 mg/L 0.3 104 20 85-115 <br /> QC Batch ID: BZJ1655 Used client sample: Y-Description: OB-22, 10/11/2016 14:14 <br /> Total Kjeldahl Nitrogen DUP 1628545-11 0.21590 0.25820 mg/L 17.8 20 <br /> MS 1628545-11 0.21590 2.4272 mg/L 90-110 <br /> MSD 1628545-11 0.21590 2.4101 mg/L 0.7 20 90-110 <br /> The results in this report apply to the samples analyzed in accordance with the chain of custody document.This analytical report must be reproduced in its entirety. <br /> All results listed in this report are for the exclusive use of the submitting party. BC Laboratories,Inc.assumes no responsibility for report alteration,separation,detachment or third party interpretation. <br /> Report ID: 1000538621 4100 Atlas Court Bakersfield,CA 93308 (661)327-4911 FAX(661)327-1918 www.bclabs.com Page 55 of 59 <br />