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Quality Control Results <br />Job Number: 720-1067-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/29/2005 1504 <br />12/29/2005 1532 <br />Laboratory Control/ <br />Laboratory Control Duplicate Recovery Report - Batch: 720-3679 <br />1.0 <br />1.0 <br />Solid <br />LCS Lab Sample ID: <br />LCSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Date Prepared: <br />Units: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />mg/Kg <br />12/28/2005 1910 <br />Prep Batch: 720-3679 <br />Analysis Batch: 720-3770 <br />d:\data\200512\122905\LCS <br />30.39 g <br />1 mL <br />d:\data\200512\122905\LCSD <br />30.12 g <br />1 mL <br />mg/Kg <br />12/28/2005 1910 <br />Analysis Batch: 720-3770 <br />Prep Batch: 720-3679 <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />LCS 720-3679/2-A <br />LCSD 720-3679/3-A <br />Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS <br />% Rec. <br />8484 21 - 133 1 35Naphthalene <br />9292 33 - 145 1 35Acenaphthylene <br />8585 47 - 145 1 35Acenaphthene <br />8484 59 - 121 1 35Fluorene <br />102102 10 - 130 1 35Phenanthrene <br />9093 27 - 133 3 35Anthracene <br />9493 26 - 137 2 35Fluoranthene <br />102116 52 - 115 12 35 *Pyrene <br />97106 33 - 143 8 35Benzo[a]anthracene <br />107121 17 - 168 11 35Chrysene <br />103106 24 - 159 2 35Benzo[b]fluoranthene <br />10096 11 - 162 5 35Benzo[k]fluoranthene <br />103104 17 - 163 0 35Benzo[a]pyrene <br />108107 9 - 171 3 35Indeno[1,2,3-cd]pyrene <br />113105 9 - 219 8 35Benzo[g,h,i]perylene <br />9498 10 - 130 3 352-Methylnaphthalene <br />111109 10 - 130 3 35Dibenz(a,h)anthracene <br />Surrogate LCS % Rec LCSD % Rec Acceptance Limits <br />Nitrobenzene-d5 83 84 23 - 120 <br />2-Fluorobiphenyl 76 74 30 - 115 <br />Terphenyl-d14 100 92 18 - 137 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 20 of 25