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Quality Control Results <br />Job Number: 720-1067-1Client: Kennedy/Jenks Consultants <br />Date Analyzed: <br />Date Analyzed: <br />Dilution: <br />Dilution: <br />12/29/2005 2037 <br />12/29/2005 2104 <br />Solid <br />Matrix Spike/ <br />Matrix Spike Duplicate Recovery Report - Batch: 720-3679 <br />1.0 <br />1.0 <br />MS Lab Sample ID: <br />MSD Lab Sample ID: <br />Client Matrix: <br />Date Prepared: <br />Date Prepared: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Instrument ID: <br />Lab File ID: <br />Initial Weight/Volume: <br />Final Weight/Volume: <br />Injection Volume: <br />Client Matrix:Solid <br />Analysis Batch: 720-3770 <br />Analysis Batch: 720-3770 <br />12/28/2005 1910 <br />12/28/2005 1910 <br />Prep Batch: 720-3679 <br />Prep Batch: 720-3679 <br />d:\data\200512\122905\720-1 <br />30.37 g <br />1 mL <br />d:\data\200512\122905\720-10 <br />30.09 g <br />1 mL <br />Method: 8270C <br />Preparation: 3550B <br />Sat 2K1 <br />Sat 2K1 <br />720-1067-5 <br />720-1067-5 <br />Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS <br />% Rec. <br />68 81 21 - 133 18 35Naphthalene <br />86 88 33 - 145 3 35Acenaphthylene <br />73 86 47 - 145 17 35Acenaphthene <br />84 76 59 - 121 10 35Fluorene <br />88 93 10 - 130 6 35Phenanthrene <br />83 87 27 - 133 6 35Anthracene <br />83 87 26 - 137 6 35Fluoranthene <br />95 104 52 - 115 10 35Pyrene <br />84 94 33 - 143 12 35Benzo[a]anthracene <br />96 107 17 - 168 12 35Chrysene <br />85 94 24 - 159 11 35Benzo[b]fluoranthene <br />83 93 11 - 162 13 35Benzo[k]fluoranthene <br />82 93 17 - 163 14 35Benzo[a]pyrene <br />86 99 9 - 171 15 35Indeno[1,2,3-cd]pyrene <br />85 96 9 - 219 13 35Benzo[g,h,i]perylene <br />79 89 10 - 130 13 352-Methylnaphthalene <br />91 106 10 - 130 16 35Dibenz(a,h)anthracene <br />Surrogate MS % Rec MSD % Rec Acceptance Limits <br />Nitrobenzene-d5 66 81 23 - 120 <br />2-Fluorobiphenyl 64 75 30 - 115 <br />Terphenyl-d14 74 89 18 - 137 <br />STL San Francisco <br />Calculations are performed before rounding to avoid round-off errors in calculated results. <br />Page 21 of 25